(E)-2-((benzyloxy)methyl)-4-ethyl-6-methoxyquinoline-3-carbaldehyde oxime

Base Information

Chemical Name:(E)-2-((benzyloxy)methyl)-4-ethyl-6-methoxyquinoline-3-carbaldehyde oxime
CAS No.:1335104-67-0
Molecular Formula:C₂₁H₂₂N₂O₃
Molecular Weight:350.417
Hs Code.:

Synonyms:(E)-2-((benzyloxy)methyl)-4-ethyl-6-methoxyquinoline-3-carbaldehyde oxime

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Chemical Property of (E)-2-((benzyloxy)methyl)-4-ethyl-6-methoxyquinoline-3-carbaldehyde oxime

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Technology Process of (E)-2-((benzyloxy)methyl)-4-ethyl-6-methoxyquinoline-3-carbaldehyde oxime

There total 5 articles about (E)-2-((benzyloxy)methyl)-4-ethyl-6-methoxyquinoline-3-carbaldehyde oxime which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 94.0%

: 1335104-66-9
2-((benzyloxy)methyl)-4-ethyl-6-methoxyquinoline-3-carbaldehyde

: 1335104-67-0
(E)-2-((benzyloxy)methyl)-4-ethyl-6-methoxyquinoline-3-carbaldehyde oxime

Guidance literature:: With hydroxylamine hydrochloride; sodium hydrogencarbonate; In ethanol; at 20 ℃; for 1h; Inert atmosphere;
DOI:10.1002/chem.201101389

Reference yield:

: 1335104-65-8
(2-((benzyloxy)methyl)-4-ethyl-6-methoxyquinolin-3-yl)methanol

: 1335104-67-0
(E)-2-((benzyloxy)methyl)-4-ethyl-6-methoxyquinoline-3-carbaldehyde oxime

Guidance literature:: Multi-step reaction with 2 steps

1: sodium hydrogencarbonate; Dess-Martin periodane / dichloromethane / 20 °C / Inert atmosphere

2: hydroxylamine hydrochloride; sodium hydrogencarbonate / ethanol / 1 h / 20 °C / Inert atmosphere

With hydroxylamine hydrochloride; sodium hydrogencarbonate; Dess-Martin periodane; In ethanol; dichloromethane;
DOI:10.1002/chem.201101389

Reference yield:

: 60997-56-0
2'-amino-5'-methoxypropiophenone

: 1335104-67-0
(E)-2-((benzyloxy)methyl)-4-ethyl-6-methoxyquinoline-3-carbaldehyde oxime

Guidance literature:: Multi-step reaction with 4 steps

1: iron(III) chloride / ethanol / 15 h / 20 °C / Inert atmosphere

2: lithium aluminium tetrahydride / diethyl ether / 0.5 h / 0 °C / Inert atmosphere

3: sodium hydrogencarbonate; Dess-Martin periodane / dichloromethane / 20 °C / Inert atmosphere

4: hydroxylamine hydrochloride; sodium hydrogencarbonate / ethanol / 1 h / 20 °C / Inert atmosphere

With iron(III) chloride; lithium aluminium tetrahydride; hydroxylamine hydrochloride; sodium hydrogencarbonate; Dess-Martin periodane; In diethyl ether; ethanol; dichloromethane;
DOI:10.1002/chem.201101389