3-N-benzylamino-2-(p-benzyloxyphenyl)-2-methyltetrahydro-2H-pyran-3-ylcarbonitrile

Base Information

Chemical Name:3-N-benzylamino-2-(p-benzyloxyphenyl)-2-methyltetrahydro-2H-pyran-3-ylcarbonitrile
CAS No.:117056-77-6
Molecular Formula:C₂₇H₂₈N₂O₂
Molecular Weight:412.532
Hs Code.:

Synonyms:3-N-benzylamino-2-(p-benzyloxyphenyl)-2-methyltetrahydro-2H-pyran-3-ylcarbonitrile

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 3-N-benzylamino-2-(p-benzyloxyphenyl)-2-methyltetrahydro-2H-pyran-3-ylcarbonitrile

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Technology Process of 3-N-benzylamino-2-(p-benzyloxyphenyl)-2-methyltetrahydro-2H-pyran-3-ylcarbonitrile

There total 2 articles about 3-N-benzylamino-2-(p-benzyloxyphenyl)-2-methyltetrahydro-2H-pyran-3-ylcarbonitrile which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 96.0%

: 151-50-8
potassium cyanide

: 117056-73-2
2-(p-benzyloxyphenyl)-2-methyltetrahydro-2H-pyran-3-one

: 100-46-9
benzylamine

: 117056-77-6
3-N-benzylamino-2-(p-benzyloxyphenyl)-2-methyltetrahydro-2H-pyran-3-ylcarbonitrile

Guidance literature:: With acetic acid; In methanol; at 60 ℃; for 20h;

Reference yield:

: 106281-29-2
5,6-dihydro-6-(p-benzyloxyphenyl)-6-methyl-5-oxo-2H-pyran-2-yl, ethyl carbonate

: 117056-77-6
3-N-benzylamino-2-(p-benzyloxyphenyl)-2-methyltetrahydro-2H-pyran-3-ylcarbonitrile

Guidance literature:: Multi-step reaction with 2 steps

1: 59 percent / H₂ / 10percent Pd/C / ethyl acetate / 760 Torr / Ambient temperature

2: 96 percent / acetic acid / methanol / 20 h / 60 °C

With hydrogen; acetic acid; palladium on activated charcoal; In methanol; ethyl acetate;