C₃₈H₅₉NO₁₂

Base Information Edit

Chemical Name:C₃₈H₅₉NO₁₂
CAS No.:922166-90-3
Molecular Formula:C₃₈H₅₉NO₁₂
Molecular Weight:721.886
Hs Code.:
Mol file:922166-90-3.mol

C<sub>38</sub>H<sub>59</sub>NO<sub>12</sub>

Synonyms:C₃₈H₅₉NO₁₂

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Chemical Property of C₃₈H₅₉NO₁₂ Edit

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Technology Process of C₃₈H₅₉NO₁₂

There total 27 articles about C₃₈H₅₉NO₁₂ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 72.0%

: 922166-88-9
(E)-(3S,4S,7S,8R,9S,11S,12R)-12-[3-bis(tert-butoxycarbonyl)amino-2,5-dimethoxyphenyl]-3,8,9,12-tetramethoxy-5,7,11-trimethyldodeca-1,5-dien-4-yl acrylate

: 922166-90-3
C₃₈H₅₉NO₁₂

Guidance literature:: With tricyclohexylphosphine[1,3-bis(2,4,6-trimethylphenyl)-4,5-dihydroimidazol-2-ylidine][benzylidene]ruthenium(II) dichloride; In toluene; for 2h; Heating;
DOI:10.1021/ol062642i

Reference yield:

: 922166-82-3
N,N-diallyl-3-bromo-2,5-dimethoxyaniline

: 922166-90-3
C₃₈H₅₉NO₁₂

Guidance literature:: Multi-step reaction with 7 steps

1: 54 percent / n-BuLi / diethyl ether; hexane / 1.5 h / -78 °C

2: 100 percent / NaH / dimethylformamide / 0 - 20 °C

3: 97 percent / N,N-dimethylbarbituric acid; Pd(PPh₃)4 / CH₂Cl₂ / 2.5 h / Heating

4: 75 percent / Et₃N; N,N-dimethylaminopyridine / tetrahydrofuran / 6 h / Heating

5: TBAF / tetrahydrofuran / 24 h / 20 °C

6: 89 percent / diisopropylethylamine / CH₂Cl₂ / 6 h / -78 °C

7: 72 percent / second generation Grubbs catalyst / toluene / 2 h / Heating

With tricyclohexylphosphine[1,3-bis(2,4,6-trimethylphenyl)-4,5-dihydroimidazol-2-ylidine][benzylidene]ruthenium(II) dichloride; dmap; tetrakis(triphenylphosphine) palladium⁽⁰⁾; n-butyllithium; 1,3-dimethylbarbituric acid; tetrabutyl ammonium fluoride; sodium hydride; triethylamine; N-ethyl-N,N-diisopropylamine; In tetrahydrofuran; diethyl ether; hexane; dichloromethane; N,N-dimethyl-formamide; toluene;
DOI:10.1021/ol062642i

Reference yield:

: tert-butyl-(4-methoxy-2-methyl-but-3-enyloxy)-diphenyl-silane

: 922166-90-3
C₃₈H₅₉NO₁₂

Guidance literature:: Multi-step reaction with 22 steps

1.1: 4.37 mg / aq. HCl / tetrahydrofuran; CH₂Cl₂ / 3 h / 20 °C

2.1: 96 percent / (S,S)-chiral titanium complex / diethyl ether; tetrahydrofuran / 5 h / -78 °C

3.1: 97 percent / KH / tetrahydrofuran / 0 - 20 °C

4.1: 98 percent / [1,3-Mes₂-(N₂C₃H₅)]Cl₂(PCy₃)Ru=CHPh; N-allyl-N-tritylamine; diisopropylethylamine / toluene / 3.5 h / Heating

5.1: OsO₄; H₂O; N-methylmorpholine N-oxide / acetone / 16 h / 20 °C

6.1: aq. NaIO₄ / acetone / 2.5 h / 20 °C

7.1: 2.73 g / 4 Angstroem molecular sieves / toluene / 2.5 h / -78 - 0 °C

8.1: 92 percent / KH / tetrahydrofuran / 0 - 20 °C

9.1: OsO₄; H₂O; N-methylmorpholine N-oxide / acetone / 18 h / 20 °C

10.1: aq. NaIO₄ / acetone / 2.5 h / 20 °C

11.1: s-BuLi / tetrahydrofuran; cyclohexane / 4.5 h / -78 - -20 °C

11.2: 1.18 g / citric acid / tetrahydrofuran; cyclohexane; H₂O / pH 4 - 5

12.1: BF₃*Et₂O / tetrahydrofuran; cyclohexane / -78 - -5 °C

12.2: 1.49 g / ethanolamine / pentane / 2.5 h / 0 °C

13.1: 94 percent / 2,6-lutidine / CH₂Cl₂ / 10 h / -78 °C

14.1: 82 percent / NH₄F; MeOH / 9.5 h / Heating

15.1: Dess-Martin periodinane; NaHCO₃ / CH₂Cl₂ / 4 h

16.1: 54 percent / n-BuLi / diethyl ether; hexane / 1.5 h / -78 °C

17.1: 100 percent / NaH / dimethylformamide / 0 - 20 °C

18.1: 97 percent / N,N-dimethylbarbituric acid; Pd(PPh₃)4 / CH₂Cl₂ / 2.5 h / Heating

19.1: 75 percent / Et₃N; N,N-dimethylaminopyridine / tetrahydrofuran / 6 h / Heating

20.1: TBAF / tetrahydrofuran / 24 h / 20 °C

21.1: 89 percent / diisopropylethylamine / CH₂Cl₂ / 6 h / -78 °C

22.1: 72 percent / second generation Grubbs catalyst / toluene / 2 h / Heating

With tricyclohexylphosphine[1,3-bis(2,4,6-trimethylphenyl)-4,5-dihydroimidazol-2-ylidine][benzylidene]ruthenium(II) dichloride; 2,6-dimethylpyridine; hydrogenchloride; methanol; dmap; ammonium fluoride; sodium periodate; osmium(VIII) oxide; tetrakis(triphenylphosphine) palladium⁽⁰⁾; n-butyllithium; 1,3-dimethylbarbituric acid; (S,S)-chiral titanium; [1,3-Mes₂-(N₂C₃H₅)]Cl₂(PCy₃)Ru=CHPh; 4 A molecular sieve; boron trifluoride diethyl etherate; N-tritylprop-2-en-1-amine; tetrabutyl ammonium fluoride; water; sec.-butyllithium; potassium hydride; sodium hydride; sodium hydrogencarbonate; Dess-Martin periodane; 4-methylmorpholine N-oxide; triethylamine; N-ethyl-N,N-diisopropylamine; In tetrahydrofuran; diethyl ether; hexane; dichloromethane; cyclohexane; N,N-dimethyl-formamide; acetone; toluene; 11.1: Corey-Schlessinger olefination / 15.1: Dess-Martin oxidation;
DOI:10.1021/ol062642i