C₁₀H₇⁽²⁾H

Base Information

Chemical Name:C₁₀H₇⁽²⁾H
CAS No.:1601463-97-1
Molecular Formula:C₁₀H₈
Molecular Weight:129.166
Hs Code.:

C<sub>10</sub>H<sub>7</sub><sup>(2)</sup>H

Synonyms:C₁₀H₇⁽²⁾H

Suppliers and Price of C₁₀H₇⁽²⁾H

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of C₁₀H₇⁽²⁾H

Chemical Property:

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Technology Process of C₁₀H₇⁽²⁾H

There total 5 articles about C₁₀H₇⁽²⁾H which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 86.0%

: 1601464-37-2
trimethyl[(2-vinylphenyl)ethynyl]silane-d1

: 1601463-97-1
C₁₀H₇⁽²⁾H

Guidance literature:: With potassium carbonate; In methanol; at 20 ℃; for 0.5h; Inert atmosphere;
DOI:10.1002/anie.201309496

Reference yield:

: 6630-33-7
ortho-bromobenzaldehyde

: 1601463-97-1
C₁₀H₇⁽²⁾H

Guidance literature:: Multi-step reaction with 5 steps

1.1: lithium aluminium deuteride / tetrahydrofuran / 1.5 h / 0 °C / Inert atmosphere

2.1: pyridinium chlorochromate / dichloromethane / 2 h / 20 °C / Inert atmosphere

3.1: n-butyllithium / hexane; tetrahydrofuran / 0.75 h / -78 °C / Inert atmosphere

3.2: 1 h / 0 - 20 °C / Inert atmosphere

4.1: bis-triphenylphosphine-palladium(II) chloride; copper(l) iodide; triethylamine / tetrahydrofuran / 7.5 h / 0 °C / Inert atmosphere; Reflux

5.1: potassium carbonate / methanol / 0.5 h / 20 °C / Inert atmosphere

With bis-triphenylphosphine-palladium(II) chloride; copper(l) iodide; n-butyllithium; lithium aluminium deuteride; potassium carbonate; triethylamine; pyridinium chlorochromate; In tetrahydrofuran; methanol; hexane; dichloromethane; 3.1: |Wittig Olefination / 3.2: |Wittig Olefination;
DOI:10.1002/anie.201309496

Reference yield:

: 90408-77-8
α-deuterio-1-bromo-2-vinylbenzene

: 1601463-97-1
C₁₀H₇⁽²⁾H

Guidance literature:: Multi-step reaction with 2 steps

1: bis-triphenylphosphine-palladium(II) chloride; copper(l) iodide; triethylamine / tetrahydrofuran / 7.5 h / 0 °C / Inert atmosphere; Reflux

2: potassium carbonate / methanol / 0.5 h / 20 °C / Inert atmosphere

With bis-triphenylphosphine-palladium(II) chloride; copper(l) iodide; potassium carbonate; triethylamine; In tetrahydrofuran; methanol;
DOI:10.1002/anie.201309496