2,7-di-tert-butyl-5-(diphenylboryl)-4-(diphenylphosphino)-9,9-dimethylthioxanthene

Base Information

Chemical Name:2,7-di-tert-butyl-5-(diphenylboryl)-4-(diphenylphosphino)-9,9-dimethylthioxanthene
CAS No.:888733-59-3
Molecular Formula:C₄₇H₄₈BPS
Molecular Weight:686.749
Hs Code.:

Synonyms:2,7-di-tert-butyl-5-(diphenylboryl)-4-(diphenylphosphino)-9,9-dimethylthioxanthene

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Chemical Property of 2,7-di-tert-butyl-5-(diphenylboryl)-4-(diphenylphosphino)-9,9-dimethylthioxanthene

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Technology Process of 2,7-di-tert-butyl-5-(diphenylboryl)-4-(diphenylphosphino)-9,9-dimethylthioxanthene

There total 1 articles about 2,7-di-tert-butyl-5-(diphenylboryl)-4-(diphenylphosphino)-9,9-dimethylthioxanthene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 66.0%

: 888733-58-2
2,7-di-tert-butyl-5-bromo-4-(diphenylphosphino)-9,9-dimethylthioxanthene

: 5123-17-1
bromodiphenylborane

: 75-05-8,26809-02-9
acetonitrile

: 888733-59-3
2,7-di-tert-butyl-5-(diphenylboryl)-4-(diphenylphosphino)-9,9-dimethylthioxanthene

Guidance literature:: With t-BuLi; In not given; substituted thioxanthene reacted with t-BuLi; quenched with Ph2BBr; MeCNadded; ppt. dried under vac.; detd. by elem. anal. and mass spectrometry;
DOI:10.1021/om0602052

Reference yield: 87.0%

: 12107-56-1
dichloro(1,5-cyclooctadiene)palladium(II)

: 888733-59-3
2,7-di-tert-butyl-5-(diphenylboryl)-4-(diphenylphosphino)-9,9-dimethylthioxanthene

: [PdCl₂(2,7-di-tert-butyl-5-diphenylboryl-4-diphenylphosphino-9,9-dimethylthioxanthene)]

Guidance literature:: In dichloromethane; (Ar); glovebox; soln. of Pd complex and ligand in CH2Cl2 was stirred at room temp. for 1 h; evapd. (vac.); hexane added; sonicated for 1 h; filtered; washed (hexane); dried (vac.); elem. anal.;
DOI:10.1021/om800670e