(S)-3-Phenyl-3-<1-<<4-(trimethylsilyl)phenyl>methyl>-4-piperidinyl>-2,6-piperidinedione

Base Information

Chemical Name:(S)-3-Phenyl-3-<1-<<4-(trimethylsilyl)phenyl>methyl>-4-piperidinyl>-2,6-piperidinedione
CAS No.:119391-67-2
Molecular Formula:C₂₆H₃₄N₂O₂Si*ClH
Molecular Weight:471.115
Hs Code.:

Synonyms:(S)-3-Phenyl-3-<1-<<4-(trimethylsilyl)phenyl>methyl>-4-piperidinyl>-2,6-piperidinedione

Suppliers and Price of (S)-3-Phenyl-3-<1-<<4-(trimethylsilyl)phenyl>methyl>-4-piperidinyl>-2,6-piperidinedione

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of (S)-3-Phenyl-3-<1-<<4-(trimethylsilyl)phenyl>methyl>-4-piperidinyl>-2,6-piperidinedione

Chemical Property:

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Technology Process of (S)-3-Phenyl-3-<1-<<4-(trimethylsilyl)phenyl>methyl>-4-piperidinyl>-2,6-piperidinedione

There total 2 articles about (S)-3-Phenyl-3-<1-<<4-(trimethylsilyl)phenyl>methyl>-4-piperidinyl>-2,6-piperidinedione which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 69.0%

: 17903-42-3
(4-(bromomethyl)phenyl)trimethylsilane

: 115216-87-0
(S)-(+)-3-Phenyl-3-(4-piperidinyl)-2,6-piperidinedione

: 119391-67-2
(S)-3-Phenyl-3-<1-<<4-(trimethylsilyl)phenyl>methyl>-4-piperidinyl>-2,6-piperidinedione

Guidance literature:: With hydrogenchloride; sodium carbonate; 1) EtOH, reflux, 0.5 h;
DOI:10.1021/jm00125a021

Reference yield:

: 21888-98-2
[125I]-Dexetimide

: 119391-67-2
(S)-3-Phenyl-3-<1-<<4-(trimethylsilyl)phenyl>methyl>-4-piperidinyl>-2,6-piperidinedione

Guidance literature:: Multi-step reaction with 2 steps

1: 93 percent / H₂, conc. aq. HCl / 5percent Pd/C / methanol / 72 h / 3102.9 Torr / Ambient temperature

2: 69 percent / 1) Na₂CO₃, 2) aq. HCl / 1) EtOH, reflux, 0.5 h

With hydrogenchloride; hydrogen; sodium carbonate; palladium on activated charcoal; In methanol;
DOI:10.1021/jm00125a021

Reference yield:

: 119391-67-2
(S)-3-Phenyl-3-<1-<<4-(trimethylsilyl)phenyl>methyl>-4-piperidinyl>-2,6-piperidinedione

: 162661-31-6
<76Br>4-bromodexetimide

Guidance literature:: With hydrogenchloride; ammonium ⁷⁶Br-bromide; chloroamine-T; In methanol; for 0.25h; Ambient temperature;
DOI:10.1002/jlcr.2580360308