dicyclohexylphenylphosphine selenide

Base Information

Chemical Name:dicyclohexylphenylphosphine selenide
CAS No.:99770-94-2
Molecular Formula:C₁₈H₂₇PSe
Molecular Weight:353.346
Hs Code.:

Synonyms:dicyclohexylphenylphosphine selenide

Suppliers and Price of dicyclohexylphenylphosphine selenide

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of dicyclohexylphenylphosphine selenide

Chemical Property:

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Technology Process of dicyclohexylphenylphosphine selenide

There total 4 articles about dicyclohexylphenylphosphine selenide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 55.0%

: 20333-40-8
dibutyl diselenide

: 693-02-7
hex-1-yne

: 6476-37-5
dicyclohexylphenylphosphine

: 1032739-17-5
(1Z)-1,2-Bis(butylselanyl)-1-hexene

: 14835-66-6
Di-n-butyl selenide

: 99770-94-2
dicyclohexylphenylphosphine selenide

Guidance literature:: dibutyl diselenide; dicyclohexylphenylphosphine; With tris-(dibenzylideneacetone)dipalladium⁽⁰⁾; at 20 ℃; Inert atmosphere;

hex-1-yne; at 140 ℃; for 12h; stereoselective reaction; Inert atmosphere;
DOI:10.1002/chem.200701278

Reference yield:

: 6476-37-5
dicyclohexylphenylphosphine

: 99770-94-2
dicyclohexylphenylphosphine selenide

Guidance literature:: With selenium; at 180 ℃;
DOI:10.1021/jo01054a064

Reference yield:

: 10074-42-7
cyclohexyllithium

: 99770-94-2
dicyclohexylphenylphosphine selenide

Guidance literature:: Multi-step reaction with 2 steps

1: pentane

2: Se / 180 °C

With selenium; In pentane;
DOI:10.1021/jo01054a064