Cyclohexanecarboxaldehyde, 4-ethyl-, trans- (9CI)

Base Information

• Chemical Name: Cyclohexanecarboxaldehyde, 4-ethyl-, trans- (9CI)
• CAS No.: 167545-47-3
• Molecular Formula: C₉H₁₆O
• Molecular Weight: 140.225
• Mol file: 167545-47-3.mol

Synonyms:Cyclohexanecarboxaldehyde, 4-ethyl-, trans- (9CI)

Chemical Property of Cyclohexanecarboxaldehyde, 4-ethyl-, trans- (9CI)

Chemical Property:

• Boiling Point: 195.0±9.0 °C(Predicted)
• PSA: 17.07000
• Density: 0.931±0.06 g/cm3(Predicted)
• LogP: 2.40170

Purity/Quality:

4-Ethylcyclohexanecarbaldehyde ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of Cyclohexanecarboxaldehyde, 4-ethyl-, trans- (9CI)

There total 2 articles about Cyclohexanecarboxaldehyde, 4-ethyl-, trans- (9CI) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 91.0%

(trans-4-ethylcyclohexyl)methanol → (trans-4-ethylcyclohexyl)carbaldehyde (167545-47-3)

Guidance literature:

With silica gel; pyridinium chlorochromate; In dichloromethane; at 20 ℃; for 2h; Inert atmosphere;

DOI:10.1002/chem.202001390

Reference yield:

trans-(4-ethylcyclohexane)carboxylic acid → (trans-4-ethylcyclohexyl)carbaldehyde (167545-47-3)

Guidance literature:

Multi-step reaction with 2 steps

1: lithium aluminium tetrahydride / diethyl ether / 0 - 20 °C

2: silica gel; pyridinium chlorochromate / dichloromethane / 2 h / 20 °C / Inert atmosphere

With lithium aluminium tetrahydride; silica gel; pyridinium chlorochromate; In diethyl ether; dichloromethane;

DOI:10.1002/chem.202001390

Refernces