5-{9-[2-(2-(tert-butoxycarbonylamino)ethyl)-4-methoxyphenoxy]-4,7-dioxa-non-1-ynyl}-5'-O-benzoyl-2',3'-didehydro-2',3'-dideoxyuridine

Base Information

Chemical Name:5-{9-[2-(2-(tert-butoxycarbonylamino)ethyl)-4-methoxyphenoxy]-4,7-dioxa-non-1-ynyl}-5'-O-benzoyl-2',3'-didehydro-2',3'-dideoxyuridine
CAS No.:1239369-05-1
Molecular Formula:C₃₇H₄₃N₃O₁₁
Molecular Weight:705.762
Hs Code.:

Synonyms:5-{9-[2-(2-(tert-butoxycarbonylamino)ethyl)-4-methoxyphenoxy]-4,7-dioxa-non-1-ynyl}-5'-O-benzoyl-2',3'-didehydro-2',3'-dideoxyuridine

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Chemical Property of 5-{9-[2-(2-(tert-butoxycarbonylamino)ethyl)-4-methoxyphenoxy]-4,7-dioxa-non-1-ynyl}-5'-O-benzoyl-2',3'-didehydro-2',3'-dideoxyuridine

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Technology Process of 5-{9-[2-(2-(tert-butoxycarbonylamino)ethyl)-4-methoxyphenoxy]-4,7-dioxa-non-1-ynyl}-5'-O-benzoyl-2',3'-didehydro-2',3'-dideoxyuridine

There total 1 articles about 5-{9-[2-(2-(tert-butoxycarbonylamino)ethyl)-4-methoxyphenoxy]-4,7-dioxa-non-1-ynyl}-5'-O-benzoyl-2',3'-didehydro-2',3'-dideoxyuridine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 72.0%

: 856676-68-1
5'-benzoyl-5-iodo-d4T

: 1101872-49-4
N-(tert-butoxycarbonyl)-2-{5-methoxy-2-[2-(2-propargyloxyethoxy)ethoxy]phenyl}ethylamine

: 1239369-05-1
5-{9-[2-(2-(tert-butoxycarbonylamino)ethyl)-4-methoxyphenoxy]-4,7-dioxa-non-1-ynyl}-5'-O-benzoyl-2',3'-didehydro-2',3'-dideoxyuridine

Guidance literature:: With copper(l) iodide; tetrakis(triphenylphosphine) palladium⁽⁰⁾; triethylamine; In tetrahydrofuran; N,N-dimethyl-formamide; at 20 ℃; Inert atmosphere;
DOI:10.1016/j.bmc.2010.05.025

Reference yield:

: 1239369-05-1
5-{9-[2-(2-(tert-butoxycarbonylamino)ethyl)-4-methoxyphenoxy]-4,7-dioxa-non-1-ynyl}-5'-O-benzoyl-2',3'-didehydro-2',3'-dideoxyuridine

: C₃₂H₃₅N₃O₉

Guidance literature:: 5-{9-[2-(2-(tert-butoxycarbonylamino)ethyl)-4-methoxyphenoxy]-4,7-dioxa-non-1-ynyl}-5'-O-benzoyl-2',3'-didehydro-2',3'-dideoxyuridine; With trifluoroacetic acid; In dichloromethane; at 0 ℃; for 2h;

With N-ethyl-N,N-diisopropylamine; In dichloromethane;
DOI:10.1016/j.bmc.2010.05.025