[3,4-bis-methoxymethoxy-2-(2-trimethylsilanyl-ethoxymethoxy)-phenyl]-[2-methoxy-3-methoxymethoxy-6-(3-methyl-but-2-enyloxy)-phenyl]-methanone

Base Information

Chemical Name:[3,4-bis-methoxymethoxy-2-(2-trimethylsilanyl-ethoxymethoxy)-phenyl]-[2-methoxy-3-methoxymethoxy-6-(3-methyl-but-2-enyloxy)-phenyl]-methanone
CAS No.:280136-82-5
Molecular Formula:C₃₁H₄₆O₁₁Si
Molecular Weight:622.785
Hs Code.:

[3,4-bis-methoxymethoxy-2-(2-trimethylsilanyl-ethoxymethoxy)-phenyl]-[2-methoxy-3-methoxymethoxy-6-(3-methyl-but-2-enyloxy)-phenyl]-methanone

Synonyms:[3,4-bis-methoxymethoxy-2-(2-trimethylsilanyl-ethoxymethoxy)-phenyl]-[2-methoxy-3-methoxymethoxy-6-(3-methyl-but-2-enyloxy)-phenyl]-methanone

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Chemical Property of [3,4-bis-methoxymethoxy-2-(2-trimethylsilanyl-ethoxymethoxy)-phenyl]-[2-methoxy-3-methoxymethoxy-6-(3-methyl-but-2-enyloxy)-phenyl]-methanone

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Technology Process of [3,4-bis-methoxymethoxy-2-(2-trimethylsilanyl-ethoxymethoxy)-phenyl]-[2-methoxy-3-methoxymethoxy-6-(3-methyl-but-2-enyloxy)-phenyl]-methanone

There total 10 articles about [3,4-bis-methoxymethoxy-2-(2-trimethylsilanyl-ethoxymethoxy)-phenyl]-[2-methoxy-3-methoxymethoxy-6-(3-methyl-but-2-enyloxy)-phenyl]-methanone which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 43.0%

: 280136-77-8
2-methoxy-1-methoxymethoxy-4-(3-methyl-but-2-enyloxy)-benzene

: 280136-81-4
3,4-bis-methoxymethoxy-2-(2-trimethylsilanyl-ethoxymethoxy)-benzoic acid methyl ester

: 280136-82-5
[3,4-bis-methoxymethoxy-2-(2-trimethylsilanyl-ethoxymethoxy)-phenyl]-[2-methoxy-3-methoxymethoxy-6-(3-methyl-but-2-enyloxy)-phenyl]-methanone

Guidance literature:: With n-butyllithium; N,N,N,N,-tetramethylethylenediamine; In tetrahydrofuran; at -15 ℃;
DOI:10.1246/cl.2000.464

Reference yield:

: 824-46-4
methoxyhydroquinone

: 280136-82-5
[3,4-bis-methoxymethoxy-2-(2-trimethylsilanyl-ethoxymethoxy)-phenyl]-[2-methoxy-3-methoxymethoxy-6-(3-methyl-but-2-enyloxy)-phenyl]-methanone

Guidance literature:: Multi-step reaction with 6 steps

1: DMAP / pyridine / 20 °C

2: KOH / methanol / 0 °C

3: 74 percent / K₂CO₃ / dimethylformamide / 20 °C

4: 97 percent / KOH / methanol / 11 °C

5: 92 percent / NaH / dimethylformamide / 20 °C

6: 43 percent / n-BuLi; TMEDA / tetrahydrofuran / -15 °C

With dmap; potassium hydroxide; n-butyllithium; N,N,N,N,-tetramethylethylenediamine; sodium hydride; potassium carbonate; In tetrahydrofuran; pyridine; methanol; N,N-dimethyl-formamide; 1: Acetylation / 2: Deacetylation / 3: Alkylation / 4: Deacetylation / 5: Condensation / 6: Condensation;
DOI:10.1246/cl.2000.464

Reference yield:

: 75514-03-3
2-methoxy-p-hydroquinone diacetate

: 280136-82-5
[3,4-bis-methoxymethoxy-2-(2-trimethylsilanyl-ethoxymethoxy)-phenyl]-[2-methoxy-3-methoxymethoxy-6-(3-methyl-but-2-enyloxy)-phenyl]-methanone

Guidance literature:: Multi-step reaction with 5 steps

1: KOH / methanol / 0 °C

2: 74 percent / K₂CO₃ / dimethylformamide / 20 °C

3: 97 percent / KOH / methanol / 11 °C

4: 92 percent / NaH / dimethylformamide / 20 °C

5: 43 percent / n-BuLi; TMEDA / tetrahydrofuran / -15 °C

With potassium hydroxide; n-butyllithium; N,N,N,N,-tetramethylethylenediamine; sodium hydride; potassium carbonate; In tetrahydrofuran; methanol; N,N-dimethyl-formamide; 1: Deacetylation / 2: Alkylation / 3: Deacetylation / 4: Condensation / 5: Condensation;
DOI:10.1246/cl.2000.464