tert-butyl 3-(4-nitrophenyl)-2,4-dioxo-3-azabicyclo[3.1.0]hexane-6-carboxylate

Base Information

Chemical Name:tert-butyl 3-(4-nitrophenyl)-2,4-dioxo-3-azabicyclo[3.1.0]hexane-6-carboxylate
CAS No.:1415110-25-6
Molecular Formula:C₁₆H₁₆N₂O₆
Molecular Weight:332.313
Hs Code.:

Synonyms:tert-butyl 3-(4-nitrophenyl)-2,4-dioxo-3-azabicyclo[3.1.0]hexane-6-carboxylate

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Chemical Property of tert-butyl 3-(4-nitrophenyl)-2,4-dioxo-3-azabicyclo[3.1.0]hexane-6-carboxylate

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Technology Process of tert-butyl 3-(4-nitrophenyl)-2,4-dioxo-3-azabicyclo[3.1.0]hexane-6-carboxylate

There total 5 articles about tert-butyl 3-(4-nitrophenyl)-2,4-dioxo-3-azabicyclo[3.1.0]hexane-6-carboxylate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 100-01-6,104810-17-5
4-nitro-aniline

: 1415110-25-6
tert-butyl 3-(4-nitrophenyl)-2,4-dioxo-3-azabicyclo[3.1.0]hexane-6-carboxylate

Guidance literature:: Multi-step reaction with 3 steps

1: acetic acid / 1.5 h / 20 °C

2: sodium acetate; acetic anhydride / 4 h / 100 °C

3: 1,2-dichloro-ethane / 1.67 h / 50 °C

With sodium acetate; acetic anhydride; In acetic acid; 1,2-dichloro-ethane;
DOI:10.1002/ejoc.201200730

Reference yield:

: 5292-43-3
bromoacetic acid tert-butyl ester

: 1415110-25-6
tert-butyl 3-(4-nitrophenyl)-2,4-dioxo-3-azabicyclo[3.1.0]hexane-6-carboxylate

Guidance literature:: Multi-step reaction with 3 steps

1: acetone / 75 h / 20 °C

2: potassium carbonate; sodium hydroxide / chloroform; water / 0.33 h / 0 - 20 °C

3: 1,2-dichloro-ethane / 1.67 h / 50 °C

With potassium carbonate; sodium hydroxide; In chloroform; water; 1,2-dichloro-ethane; acetone;
DOI:10.1002/ejoc.201200730

Reference yield:

: 36342-10-6,36847-91-3,37904-21-5
4-(4-nitrophenylamino)-4-oxobut-2-enoic acid

: 1415110-25-6
tert-butyl 3-(4-nitrophenyl)-2,4-dioxo-3-azabicyclo[3.1.0]hexane-6-carboxylate

Guidance literature:: Multi-step reaction with 2 steps

1: sodium acetate; acetic anhydride / 4 h / 100 °C

2: 1,2-dichloro-ethane / 1.67 h / 50 °C

With sodium acetate; acetic anhydride; In 1,2-dichloro-ethane;
DOI:10.1002/ejoc.201200730