(S)-ethyl 2-diazo-3-oxo-5-fenyl hexanoate

Base Information

Chemical Name:(S)-ethyl 2-diazo-3-oxo-5-fenyl hexanoate
CAS No.:1349699-22-4
Molecular Formula:C₁₄H₁₆N₂O₃
Molecular Weight:260.293
Hs Code.:

Synonyms:(S)-ethyl 2-diazo-3-oxo-5-fenyl hexanoate

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of (S)-ethyl 2-diazo-3-oxo-5-fenyl hexanoate

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Technology Process of (S)-ethyl 2-diazo-3-oxo-5-fenyl hexanoate

There total 2 articles about (S)-ethyl 2-diazo-3-oxo-5-fenyl hexanoate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 79.0%

: 1349699-08-6
(S)-ethyl 3-oxo-5-phenylhexanoate

: 1349699-22-4
(S)-ethyl 2-diazo-3-oxo-5-fenyl hexanoate

Guidance literature:: With 4-acetamidobenzenesulfonyl azide; 1,8-diazabicyclo[5.4.0]undec-7-ene; at 20 ℃; for 4h; Inert atmosphere;
DOI:10.1021/ol202968z

Reference yield:

: C₁₅H₁₇NO₃S

: 1349699-22-4
(S)-ethyl 2-diazo-3-oxo-5-fenyl hexanoate

Guidance literature:: Multi-step reaction with 2 steps

1: 1H-imidazole; magnesium chloride / tetrahydrofuran / 16 h / 20 °C / Inert atmosphere

2: 4-acetamidobenzenesulfonyl azide; 1,8-diazabicyclo[5.4.0]undec-7-ene / 4 h / 20 °C / Inert atmosphere

With 1H-imidazole; 4-acetamidobenzenesulfonyl azide; 1,8-diazabicyclo[5.4.0]undec-7-ene; magnesium chloride; In tetrahydrofuran;
DOI:10.1021/ol202968z