[5-(4,7-dimethoxynaphth-1-yl)-10,15,20-tris(3,5-difluorophenyl)porphyrinato]nickel(II)

Base Information

Chemical Name:[5-(4,7-dimethoxynaphth-1-yl)-10,15,20-tris(3,5-difluorophenyl)porphyrinato]nickel(II)
CAS No.:1350372-44-9
Molecular Formula:C₅₀H₂₈F₆N₄NiO₂
Molecular Weight:889.478
Hs Code.:

Synonyms:[5-(4,7-dimethoxynaphth-1-yl)-10,15,20-tris(3,5-difluorophenyl)porphyrinato]nickel(II)

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Chemical Property of [5-(4,7-dimethoxynaphth-1-yl)-10,15,20-tris(3,5-difluorophenyl)porphyrinato]nickel(II)

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Technology Process of [5-(4,7-dimethoxynaphth-1-yl)-10,15,20-tris(3,5-difluorophenyl)porphyrinato]nickel(II)

There total 4 articles about [5-(4,7-dimethoxynaphth-1-yl)-10,15,20-tris(3,5-difluorophenyl)porphyrinato]nickel(II) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 99.0%

: 5-(4,7-dimethoxynaphth-1-yl)-10,15,20-tris(3,5-difluorophenyl)porphyrin

: 1350372-44-9
[5-(4,7-dimethoxynaphth-1-yl)-10,15,20-tris(3,5-difluorophenyl)porphyrinato]nickel(II)

Guidance literature:: With bis(acetylacetonate)nickel(II); In toluene; at 100 ℃; for 5h;
DOI:10.1039/c1ob06281f

Reference yield: 99.0%

: (3,5-F₂C₆H₃)3((MeO)2C₁₀H₅)C₂₀H₁₀N₄

: 3264-82-2
nickel(II) acetylacetonate

: 1350372-44-9
[5-(4,7-dimethoxynaphth-1-yl)-10,15,20-tris(3,5-difluorophenyl)porphyrinato]nickel(II)

Guidance literature:: In toluene; reaction of nickel compd. with porphyrin deriv. in toluene at 100°C for 5 h;
DOI:10.1039/c1ob06281f

Reference yield:

: 90381-44-5
4,7-dimethoxy-1-naphthaldehyde

: 1350372-44-9
[5-(4,7-dimethoxynaphth-1-yl)-10,15,20-tris(3,5-difluorophenyl)porphyrinato]nickel(II)

Guidance literature:: Multi-step reaction with 2 steps

1.1: boron trifluoride diethyl etherate / chloroform / 1.5 h / 20 °C

1.2: 0.25 h

2.1: bis(acetylacetonate)nickel(II) / toluene / 5 h / 100 °C

With bis(acetylacetonate)nickel(II); boron trifluoride diethyl etherate; In chloroform; toluene;
DOI:10.1039/c1ob06281f