2(R)-{2-[(1H-indole-2-carbonyl)amino]benzoylamino}-4-methylsulfanylbutyric acid ethyl ester

Base Information

Chemical Name:2(R)-{2-[(1H-indole-2-carbonyl)amino]benzoylamino}-4-methylsulfanylbutyric acid ethyl ester
CAS No.:1155261-62-3
Molecular Formula:C₂₃H₂₅N₃O₄S
Molecular Weight:439.535
Hs Code.:

Synonyms:2(R)-{2-[(1H-indole-2-carbonyl)amino]benzoylamino}-4-methylsulfanylbutyric acid ethyl ester

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Chemical Property of 2(R)-{2-[(1H-indole-2-carbonyl)amino]benzoylamino}-4-methylsulfanylbutyric acid ethyl ester

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Technology Process of 2(R)-{2-[(1H-indole-2-carbonyl)amino]benzoylamino}-4-methylsulfanylbutyric acid ethyl ester

There total 1 articles about 2(R)-{2-[(1H-indole-2-carbonyl)amino]benzoylamino}-4-methylsulfanylbutyric acid ethyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 80.0%

Indole-2-carboxylic acid: 1477-50-5,1228050-17-6
Indole-2-carboxylic acid

: 1155261-39-4
2-(R)-(2-aminobenzoylamino)-4-methylsulfanylbutyric acid ethyl ester

: 1155261-62-3
2(R)-{2-[(1H-indole-2-carbonyl)amino]benzoylamino}-4-methylsulfanylbutyric acid ethyl ester

Guidance literature:: Indole-2-carboxylic acid; With phosphorus pentachloride; acetyl chloride; at 20 ℃; for 3.5h; Cooling with ice;

2-(R)-(2-aminobenzoylamino)-4-methylsulfanylbutyric acid ethyl ester; With pyridine; In dichloromethane; at 0 - 20 ℃;
DOI:10.1016/j.bmc.2009.02.012

Reference yield: 61.0%

: 1155261-62-3
2(R)-{2-[(1H-indole-2-carbonyl)amino]benzoylamino}-4-methylsulfanylbutyric acid ethyl ester

: 1155261-75-8
2-(R)-{2-[(1H-indole-2-carbonyl)amino]benzoylamino}-4-methylsulfanylbutyric acid

Guidance literature:: 2(R)-{2-[(1H-indole-2-carbonyl)amino]benzoylamino}-4-methylsulfanylbutyric acid ethyl ester; With lithium hydroxide monohydrate; water; In tetrahydrofuran; at 20 ℃; for 24h;

With hydrogenchloride; In tetrahydrofuran; water;
DOI:10.1016/j.bmc.2009.02.012