carbamic acid 3-[4-(3,4-dimethoxy-phenyl)-piperazine-1-yl]-1-phenyl-butyl ester

Base Information

Chemical Name:carbamic acid 3-[4-(3,4-dimethoxy-phenyl)-piperazine-1-yl]-1-phenyl-butyl ester
CAS No.:1083076-53-2
Molecular Formula:C₂₃H₃₁N₃O₄
Molecular Weight:413.517
Hs Code.:

Synonyms:carbamic acid 3-[4-(3,4-dimethoxy-phenyl)-piperazine-1-yl]-1-phenyl-butyl ester

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Chemical Property of carbamic acid 3-[4-(3,4-dimethoxy-phenyl)-piperazine-1-yl]-1-phenyl-butyl ester

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Technology Process of carbamic acid 3-[4-(3,4-dimethoxy-phenyl)-piperazine-1-yl]-1-phenyl-butyl ester

There total 6 articles about carbamic acid 3-[4-(3,4-dimethoxy-phenyl)-piperazine-1-yl]-1-phenyl-butyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 22.0%

: 495-40-9
propiophenone

: 16015-73-9
1-(3,4-dimethoxyphenyl)piperazine

: 530-62-1
1,1'-carbonyldiimidazole

: 1083076-53-2
carbamic acid 3-[4-(3,4-dimethoxy-phenyl)-piperazine-1-yl]-1-phenyl-butyl ester

Guidance literature:: propiophenone; 1-(3,4-dimethoxyphenyl)piperazine; In ethanol; at 72 ℃; for 48h;

With methanol; sodium tetrahydroborate; at 20 ℃; for 2h;

1,1'-carbonyldiimidazole; Further stages;

Reference yield:

: C₂₂H₃₀N₂O₃

: 530-62-1
1,1'-carbonyldiimidazole

: 1083076-53-2
carbamic acid 3-[4-(3,4-dimethoxy-phenyl)-piperazine-1-yl]-1-phenyl-butyl ester

Guidance literature:: C₂₂H₃₀N₂O₃; 1,1'-carbonyldiimidazole; In tetrahydrofuran; at 20 ℃; for 1h;

With ammonium hydroxide; In tetrahydrofuran; at 20 ℃; for 2h;

Reference yield:

: 16015-73-9
1-(3,4-dimethoxyphenyl)piperazine

: 1083076-53-2
carbamic acid 3-[4-(3,4-dimethoxy-phenyl)-piperazine-1-yl]-1-phenyl-butyl ester

Guidance literature:: Multi-step reaction with 3 steps

1.1: ethanol / 48 h / 72 °C

2.1: sodium tetrahydroborate / methanol / 2 h / 20 °C

3.1: tetrahydrofuran / 1 h / 20 °C

3.2: 2 h / 20 °C

With sodium tetrahydroborate; In tetrahydrofuran; methanol; ethanol;