Technology Process of C24H31N5O5
There total 7 articles about C24H31N5O5 which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
With
hydrogen; palladium;
In
methanol;
for 24h;
- Guidance literature:
-
Multi-step reaction with 5 steps
1: hydrogenchloride / methanol / 1 h
2: N-ethyl-N,N-diisopropylamine / acetonitrile / Reflux
3: dmap; triethylamine / tetrahydrofuran / Reflux
4: potassium phosphate; tetrakis(triphenylphosphine) palladium(0); XPhos / 1,4-dioxane; water / 18 h / 80 °C / Inert atmosphere
5: hydrogen; palladium / methanol / 24 h
With
hydrogenchloride; dmap; potassium phosphate; tetrakis(triphenylphosphine) palladium(0); hydrogen; palladium; triethylamine; N-ethyl-N,N-diisopropylamine; XPhos;
In
tetrahydrofuran; 1,4-dioxane; methanol; water; acetonitrile;
4: |Suzuki Coupling;
- Guidance literature:
-
Multi-step reaction with 4 steps
1: N-ethyl-N,N-diisopropylamine / acetonitrile / Reflux
2: dmap; triethylamine / tetrahydrofuran / Reflux
3: potassium phosphate; tetrakis(triphenylphosphine) palladium(0); XPhos / 1,4-dioxane; water / 18 h / 80 °C / Inert atmosphere
4: hydrogen; palladium / methanol / 24 h
With
dmap; potassium phosphate; tetrakis(triphenylphosphine) palladium(0); hydrogen; palladium; triethylamine; N-ethyl-N,N-diisopropylamine; XPhos;
In
tetrahydrofuran; 1,4-dioxane; methanol; water; acetonitrile;
3: |Suzuki Coupling;