9-((N-methyl-N-(o-boronobenzyl)amino)methyl)-10-((N-methyl-N-(bromoacetyl)amino)methyl)anthracene

Base Information

• Chemical Name: 9-((N-methyl-N-(o-boronobenzyl)amino)methyl)-10-((N-methyl-N-(bromoacetyl)amino)methyl)anthracene
• CAS No.: 501120-75-8
• Molecular Formula: C₂₇H₂₈BBrN₂O₃
• Molecular Weight: 519.246

Synonyms:9-((N-methyl-N-(o-boronobenzyl)amino)methyl)-10-((N-methyl-N-(bromoacetyl)amino)methyl)anthracene

Chemical Property of 9-((N-methyl-N-(o-boronobenzyl)amino)methyl)-10-((N-methyl-N-(bromoacetyl)amino)methyl)anthracene

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of 9-((N-methyl-N-(o-boronobenzyl)amino)methyl)-10-((N-methyl-N-(bromoacetyl)amino)methyl)anthracene

There total 3 articles about 9-((N-methyl-N-(o-boronobenzyl)amino)methyl)-10-((N-methyl-N-(bromoacetyl)amino)methyl)anthracene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 82.0%

2-Bromoacetyl bromide (598-21-0) + 9-((N-methyl-N-(o-boronobenzyl)amino)methyl)-10-((methylamino)methyl)anthracene → 9-((N-methyl-N-(o-boronobenzyl)amino)methyl)-10-((N-methyl-N-(bromoacetyl)amino)methyl)anthracene (501120-75-8)

Guidance literature:

With N-ethyl-N,N-diisopropylamine; In dichloromethane; at 0 ℃; for 0.5h;

DOI:10.1021/ja035631i

Reference yield:

1,1′-(anthracene-9,10-diyl)bis(N-methylmethanamine) → 9-((N-methyl-N-(o-boronobenzyl)amino)methyl)-10-((N-methyl-N-(bromoacetyl)amino)methyl)anthracene (501120-75-8)

Guidance literature:

Multi-step reaction with 2 steps

1: 18 percent / K₂CO₃ / tetrahydrofuran / 3 h / Heating

2: 82 percent / DIEA / CH₂Cl₂ / 0.5 h / 0 °C

With potassium carbonate; N-ethyl-N,N-diisopropylamine; In tetrahydrofuran; dichloromethane;

DOI:10.1021/ja035631i

Reference yield:

2-{2-(bromomethyl)phenyl}-1,3,2-dioxaborolane (80137-75-3) → 9-((N-methyl-N-(o-boronobenzyl)amino)methyl)-10-((N-methyl-N-(bromoacetyl)amino)methyl)anthracene (501120-75-8)

Guidance literature:

Multi-step reaction with 2 steps

1: 18 percent / K₂CO₃ / tetrahydrofuran / 3 h / Heating

2: 82 percent / DIEA / CH₂Cl₂ / 0.5 h / 0 °C

With potassium carbonate; N-ethyl-N,N-diisopropylamine; In tetrahydrofuran; dichloromethane;

DOI:10.1021/ja035631i

upstream raw materials:

2-Bromoacetyl bromide

2-{2-(bromomethyl)phenyl}-1,3,2-dioxaborolane

Post a RFQ

Cas No.:

Product Name:

Quantity:

Please select Metric Ton KG G Pound L ML

Email:

Company name:

Valid Period:

Detailed Requirements:

• Sample
• MOQ
• GMP
• FDA
• Price
  FOB CIF CFR EXW
• Urgent purchase

Enter 15 to 2000 letters.Word count: 0 letters

Attach files(File Format: Jpeg, Jpg, Gif, Png, PDF, PPT, Zip, Rar,Word or Excel Maximum File Size: 3MB)

Remove

Submit

1

What can I do for you?
Get Best Price

Get Best Price for 501120-75-8 9-((N-methyl-N-(o-boronobenzyl)amino)methyl)-10-((N-methyl-N-(bromoacetyl)amino)methyl)anthracene

Send

Send

Metric Ton KG G Pound L ML

Send

Send