trans-{Os(2,2'-bipyridine)(PPh₃)2(CO)H}PF₆

Base Information

• Chemical Name: trans-{Os(2,2'-bipyridine)(PPh₃)2(CO)H}PF₆
• CAS No.: 84117-37-3
• Molecular Formula: C₄₇H₃₉N₂OOsP₂*F₆P
• Molecular Weight: 1044.95

Synonyms:trans-{Os(2,2'-bipyridine)(PPh₃)2(CO)H}PF₆

Chemical Property of trans-{Os(2,2'-bipyridine)(PPh₃)2(CO)H}PF₆

Chemical Property:

Purity/Quality:

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Technology Process of trans-{Os(2,2'-bipyridine)(PPh₃)2(CO)H}PF₆

There total 6 articles about trans-{Os(2,2'-bipyridine)(PPh₃)2(CO)H}PF₆ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 70.0%

cis-{Os(2,2'-bipyridine)2(CO)Cl}(PF6) (80502-54-1) → cis-{Os(2,2'-bipyridine)2(CO)H} hexafluorophosphate (84117-35-1) + trans-{Os(2,2'-bipyridine)(PPh3)2(CO)H}PF6 (84117-37-3)

Guidance literature:

With triphenylphosphine or 2,6-lutidine; In ethylene glycol; The complex was allowed to reats with PPh3 or 2,6-lutidine in ethalene glycol at reflux for 12 h;; chromy.;;

DOI:10.1021/om00086a016

Reference yield:

[Os(2,2'-bypiridine)Cl4] (57288-05-8) → trans-{Os(2,2'-bipyridine)(PPh3)2(CO)H}PF6 (84117-37-3)

Guidance literature:

With triphenylphosphine; In ethylene glycol; 1 equiv of complex, 4 equiv of PPh3, ethylene glycol, reflux, 15 min;;

DOI:10.1021/om00086a016

Reference yield:

cis-{Os(2,2'-bipyridine)2(CO)Cl}(PF6) (80502-54-1) → trans-{Os(2,2'-bipyridine)(PPh3)2(CO)H}PF6 (84117-37-3)

Guidance literature:

With triphenylphosphine; In ethylene glycol; Prolonged reflux of complex in ethylene glycol with PPh3;;

DOI:10.1021/om00086a016

upstream raw materials:

cis-{Os(2,2'-bipyridine)2(CO)Cl}(PF₆)

potassium hexafluorophosphate

OsHCl(CO)(triphenylphosphine)₃

[Os(2,2'-bypiridine)Cl₄]

Downstream raw materials:

{Os(C₅H₄N)2(P(C₆H₅)3)2(CO)H₂}⁽²⁺⁾

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