1-{3-[(2E)-3,7-dimethylocta-2,6-dien-1-yl]-2-hydroxy-4-(methoxymethoxy)phenyl}ethanone

Base Information

• Chemical Name: 1-{3-[(2E)-3,7-dimethylocta-2,6-dien-1-yl]-2-hydroxy-4-(methoxymethoxy)phenyl}ethanone
• CAS No.: 1219966-99-0
• Molecular Formula: C₂₀H₂₈O₄
• Molecular Weight: 332.44

Synonyms:1-{3-[(2E)-3,7-dimethylocta-2,6-dien-1-yl]-2-hydroxy-4-(methoxymethoxy)phenyl}ethanone

Chemical Property of 1-{3-[(2E)-3,7-dimethylocta-2,6-dien-1-yl]-2-hydroxy-4-(methoxymethoxy)phenyl}ethanone

Chemical Property:

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Technology Process of 1-{3-[(2E)-3,7-dimethylocta-2,6-dien-1-yl]-2-hydroxy-4-(methoxymethoxy)phenyl}ethanone

There total 1 articles about 1-{3-[(2E)-3,7-dimethylocta-2,6-dien-1-yl]-2-hydroxy-4-(methoxymethoxy)phenyl}ethanone which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 80.0%

1-{3-[(2E)-3,7-dimethylocta-2,6-dien-1-yl]-2,4-dihydroxyphenyl}ethanone (20212-67-3) + chloromethyl methyl ether (107-30-2) → 1-{3-[(2E)-3,7-dimethylocta-2,6-dien-1-yl]-2-hydroxy-4-(methoxymethoxy)phenyl}ethanone (1219966-99-0)

Guidance literature:

With triisopropylamine; In dichloromethane; at 20 ℃; for 4h; Inert atmosphere;

DOI:10.1002/hlca.200900251

Reference yield: 73.0%

3,4-bis{[2-(trimethylsilyl)ethoxy]methoxy}benzaldehyde (1028149-22-5) + 1-{3-[(2E)-3,7-dimethylocta-2,6-dien-1-yl]-2-hydroxy-4-(methoxymethoxy)phenyl}ethanone (1219966-99-0) → (2E)-3-{3,4-Bis{[2-(trimethylsilyl)ethoxy]methoxy}phenyl}-1-[5-hydroxy-2-methyl-2-(4-methylpent-3-en-1-yl)-2H-chromen-6-yl]prop-2-en-1-one (1229515-85-8)

Guidance literature:

With potassium hydroxide; In ethanol; at 20 ℃; for 48h; Inert atmosphere;

DOI:10.1002/hlca.200900251

Reference yield: 70.0%

1-{3-[(2E)-3,7-dimethylocta-2,6-dien-1-yl]-2-hydroxy-4-(methoxymethoxy)phenyl}ethanone (1219966-99-0) + 4-β-(trimethylsilyl)ethoxymethoxybenzaldehyde → (2E)-1-[3-geranyl-2-hydroxy-4-(methoxymethoxy)phenyl]-3-{4-{[2-(trimethylsilyl)ethoxy]methoxy}-phenyl}prop-2-en-1-one (1229515-77-8)

Guidance literature:

With potassium hydroxide; In ethanol; at 20 ℃; for 48h; Inert atmosphere;

DOI:10.1002/hlca.200900251

upstream raw materials:

1-{3-[(2E)-3,7-dimethylocta-2,6-dien-1-yl]-2,4-dihydroxyphenyl}ethanone

chloromethyl methyl ether

Downstream raw materials:

(2E)-3-{3,4-bis{[2-(trimethylsilyl)ethoxy]methoxy}phenyl}-1-[3-geranyl-2-hydroxy-4-(methoxymethoxy)phenyl]prop-2-en-1-one

(2E)-3-{3,4-Bis{[2-(trimethylsilyl)ethoxy]methoxy}phenyl}-1-[5-hydroxy-2-methyl-2-(4-methylpent-3-en-1-yl)-2H-chromen-6-yl]prop-2-en-1-one

(2E)-1-[3-geranyl-2-hydroxy-4-(methoxymethoxy)phenyl]-3-{4-{[2-(trimethylsilyl)ethoxy]methoxy}-phenyl}prop-2-en-1-one

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