2-(2',3',4'-tri-O-benzoyl-6'-deoxy-α-L-manno-hexopyranosyl)-6-amino<1,2,4>triazolo<1,5-a>pyridine

Base Information

Chemical Name:2-(2',3',4'-tri-O-benzoyl-6'-deoxy-α-L-manno-hexopyranosyl)-6-amino<1,2,4>triazolo<1,5-a>pyridine
CAS No.:78796-92-6
Molecular Formula:C₃₃H₂₈N₄O₇
Molecular Weight:592.608
Hs Code.:

Synonyms:2-(2',3',4'-tri-O-benzoyl-6'-deoxy-α-L-manno-hexopyranosyl)-6-amino<1,2,4>triazolo<1,5-a>pyridine

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Chemical Property of 2-(2',3',4'-tri-O-benzoyl-6'-deoxy-α-L-manno-hexopyranosyl)-6-amino<1,2,4>triazolo<1,5-a>pyridine

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Technology Process of 2-(2',3',4'-tri-O-benzoyl-6'-deoxy-α-L-manno-hexopyranosyl)-6-amino<1,2,4>triazolo<1,5-a>pyridine

There total 6 articles about 2-(2',3',4'-tri-O-benzoyl-6'-deoxy-α-L-manno-hexopyranosyl)-6-amino<1,2,4>triazolo<1,5-a>pyridine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 66.0%

: 78796-89-1
2-(2',3',4'-tri-O-benzoyl-6'-deoxy-α-L-manno-hexopyranosyl)-6-nitro<1,2,4>triazolo<1,5-a>pyridine

: 78796-92-6
2-(2',3',4'-tri-O-benzoyl-6'-deoxy-α-L-manno-hexopyranosyl)-6-amino<1,2,4>triazolo<1,5-a>pyridine

Guidance literature:: With hydrogen; palladium on activated charcoal; In acetone; for 4h; under 760 Torr; Ambient temperature;
DOI:10.1021/jm00143a006

Reference yield:

: 61198-83-2,73891-00-6,73891-01-7,113567-33-2,113567-34-3,122089-70-7,135266-93-2,135266-94-3,140223-15-0,141115-69-7,148152-57-2,71155-57-2
1,2,3,4-tetra-O-benzoyl-α/β-L-rhamnopyranose

: 78796-92-6
2-(2',3',4'-tri-O-benzoyl-6'-deoxy-α-L-manno-hexopyranosyl)-6-amino<1,2,4>triazolo<1,5-a>pyridine

Guidance literature:: Multi-step reaction with 5 steps

1: 77 percent / hydrobromic acid / acetic acid / 4 °C

2: 14 percent / nitromethane / 72 h

3: 82 percent / hydrochloric acid / diethyl ether / 4 °C

4: 35 percent / pyridine / CH₂Cl₂ / 120 h / Heating

5: 66 percent / H₂ / 10percent Pd/C / acetone / 4 h / 760 Torr / Ambient temperature

With pyridine; hydrogenchloride; hydrogen bromide; hydrogen; palladium on activated charcoal; In diethyl ether; nitromethane; dichloromethane; acetic acid; acetone;
DOI:10.1021/jm00143a006

Reference yield:

: 14218-08-7,41881-44-1,53297-33-9,60820-93-1,61198-82-1,67986-91-8,73068-86-7,131897-72-8,131897-73-9
2,3,4-tri-O-benzoyl-α-L-rhamnopyranosyl bromide

: 78796-92-6
2-(2',3',4'-tri-O-benzoyl-6'-deoxy-α-L-manno-hexopyranosyl)-6-amino<1,2,4>triazolo<1,5-a>pyridine

Guidance literature:: Multi-step reaction with 4 steps

1: 14 percent / nitromethane / 72 h

2: 82 percent / hydrochloric acid / diethyl ether / 4 °C

3: 35 percent / pyridine / CH₂Cl₂ / 120 h / Heating

4: 66 percent / H₂ / 10percent Pd/C / acetone / 4 h / 760 Torr / Ambient temperature

With pyridine; hydrogenchloride; hydrogen; palladium on activated charcoal; In diethyl ether; nitromethane; dichloromethane; acetone;
DOI:10.1021/jm00143a006