(E)-2-Cyclopropyl-1-(dimethyl-phenyl-silanyl)-6,10-dimethyl-undeca-5,9-dien-2-ol

Base Information

Chemical Name:(E)-2-Cyclopropyl-1-(dimethyl-phenyl-silanyl)-6,10-dimethyl-undeca-5,9-dien-2-ol
CAS No.:714230-51-0
Molecular Formula:C₂₄H₃₈OSi
Molecular Weight:370.651
Hs Code.:

Synonyms:(E)-2-Cyclopropyl-1-(dimethyl-phenyl-silanyl)-6,10-dimethyl-undeca-5,9-dien-2-ol

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Chemical Property of (E)-2-Cyclopropyl-1-(dimethyl-phenyl-silanyl)-6,10-dimethyl-undeca-5,9-dien-2-ol

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Technology Process of (E)-2-Cyclopropyl-1-(dimethyl-phenyl-silanyl)-6,10-dimethyl-undeca-5,9-dien-2-ol

There total 3 articles about (E)-2-Cyclopropyl-1-(dimethyl-phenyl-silanyl)-6,10-dimethyl-undeca-5,9-dien-2-ol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1833-51-8
chloromethyldimethylphenylsilane

: 714230-48-5
1-cyclopropyl-5,9-dimethyl-deca-4,8-dien-1-one

: 714230-51-0
(E)-2-Cyclopropyl-1-(dimethyl-phenyl-silanyl)-6,10-dimethyl-undeca-5,9-dien-2-ol

Guidance literature:: chloromethyldimethylphenylsilane; With magnesium; In diethyl ether; for 1h;

With cerium(III) chloride; In tetrahydrofuran; diethyl ether; at 0 ℃; for 1h;

1-cyclopropyl-5,9-dimethyl-deca-4,8-dien-1-one; In tetrahydrofuran; diethyl ether; at 0 - 20 ℃;
DOI:10.1021/ol049311v

Reference yield:

: 765-43-5
Cyclopropyl methyl ketone

: 714230-51-0
(E)-2-Cyclopropyl-1-(dimethyl-phenyl-silanyl)-6,10-dimethyl-undeca-5,9-dien-2-ol

Guidance literature:: Multi-step reaction with 2 steps

1.1: lithium diisopropylamide / tetrahydrofuran / 0.5 h / -78 °C

1.2: 52 percent / tetrahydrofuran / -78 - 20 °C

2.1: Mg / diethyl ether / 1 h

2.2: cerium(III) chloride / tetrahydrofuran; diethyl ether / 1 h / 0 °C

2.3: tetrahydrofuran; diethyl ether / 0 - 20 °C

With magnesium; lithium diisopropyl amide; In tetrahydrofuran; diethyl ether;
DOI:10.1021/ol049311v

Reference yield:

: 82859-38-9
(2E)-1-iodo-3,7-dimethylocta-2,6-diene

: 714230-51-0
(E)-2-Cyclopropyl-1-(dimethyl-phenyl-silanyl)-6,10-dimethyl-undeca-5,9-dien-2-ol

Guidance literature:: Multi-step reaction with 2 steps

1.1: lithium diisopropylamide / tetrahydrofuran / 0.5 h / -78 °C

1.2: 52 percent / tetrahydrofuran / -78 - 20 °C

2.1: Mg / diethyl ether / 1 h

2.2: cerium(III) chloride / tetrahydrofuran; diethyl ether / 1 h / 0 °C

2.3: tetrahydrofuran; diethyl ether / 0 - 20 °C

With magnesium; lithium diisopropyl amide; In tetrahydrofuran; diethyl ether;
DOI:10.1021/ol049311v