C₅₁H₅₆O₁₁

Base Information

Chemical Name:C₅₁H₅₆O₁₁
CAS No.:1187445-24-4
Molecular Formula:C₅₁H₅₆O₁₁
Molecular Weight:844.999
Hs Code.:

C<sub>51</sub>H<sub>56</sub>O<sub>11</sub>

Synonyms:C₅₁H₅₆O₁₁

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Chemical Property of C₅₁H₅₆O₁₁

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Technology Process of C₅₁H₅₆O₁₁

There total 11 articles about C₅₁H₅₆O₁₁ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 89.0%

: 1187445-14-2
C₄₉H₅₄O₁₀

: 108-24-7
acetic anhydride

: 1187445-24-4
C₅₁H₅₆O₁₁

Guidance literature:: With pyridine; dmap; at 20 ℃;
DOI:10.1016/j.tetlet.2009.06.115

Reference yield:

: (2R,3R,4R,5S,6R)-1,2,4-tri-O-benzyl-1,2,3,4,5,6-hexahydroxyoct-7-ene

: 1187445-24-4
C₅₁H₅₆O₁₁

Guidance literature:: Multi-step reaction with 9 steps

1.1: pyridinium p-toluenesulfonate / 0.25 h / 20 °C

2.1: oxalyl dichloride; dimethyl sulfoxide / dichloromethane / 0.5 h / -60 °C / Inert atmosphere

2.2: -60 - 20 °C / Inert atmosphere

3.1: n-butyllithium / hexane; toluene / 0 - 20 °C / Inert atmosphere

3.2: -78 - 20 °C / Inert atmosphere

4.1: hydrogenchloride / water; acetic acid / 2.5 h / 80 °C

5.1: Hoveyda-Grubbs catalyst second generation / toluene / 1 h / 60 °C / Inert atmosphere

6.1: palladium 10% on activated carbon; hydrogen; triethylamine / ethyl acetate / 2 h / 20 °C / Inert atmosphere

7.1: di-isopropyl azodicarboxylate; triphenylphosphine / tetrahydrofuran

8.1: boron trifluoride diethyl etherate / dichloromethane / Inert atmosphere

9.1: pyridine / 3 h / 20 °C

With hydrogenchloride; n-butyllithium; Hoveyda-Grubbs catalyst second generation; oxalyl dichloride; di-isopropyl azodicarboxylate; palladium 10% on activated carbon; boron trifluoride diethyl etherate; hydrogen; pyridinium p-toluenesulfonate; dimethyl sulfoxide; triethylamine; triphenylphosphine; In tetrahydrofuran; pyridine; hexane; dichloromethane; water; acetic acid; ethyl acetate; toluene; 2.1: Swern oxidation / 2.2: Swern oxidation / 3.2: Wittig reaction / 7.1: Mitsunobu reaction;
DOI:10.1016/j.carres.2011.04.032

Reference yield:

: 35958-64-6
3,5,6-Tri-O-benzyl-D-glucofuranose

: 1187445-24-4
C₅₁H₅₆O₁₁

Guidance literature:: Multi-step reaction with 10 steps

1.1: tetrahydrofuran / 0 - 20 °C / Inert atmosphere

1.2: 0 °C / pH 7 / Inert atmosphere

2.1: pyridinium p-toluenesulfonate / 0.25 h / 20 °C

3.1: oxalyl dichloride; dimethyl sulfoxide / dichloromethane / 0.5 h / -60 °C / Inert atmosphere

3.2: -60 - 20 °C / Inert atmosphere

4.1: n-butyllithium / hexane; toluene / 0 - 20 °C / Inert atmosphere

4.2: -78 - 20 °C / Inert atmosphere

5.1: hydrogenchloride / water; acetic acid / 2.5 h / 80 °C

6.1: Hoveyda-Grubbs catalyst second generation / toluene / 1 h / 60 °C / Inert atmosphere

7.1: palladium 10% on activated carbon; hydrogen; triethylamine / ethyl acetate / 2 h / 20 °C / Inert atmosphere

8.1: di-isopropyl azodicarboxylate; triphenylphosphine / tetrahydrofuran

9.1: boron trifluoride diethyl etherate / dichloromethane / Inert atmosphere

10.1: pyridine / 3 h / 20 °C

With hydrogenchloride; n-butyllithium; Hoveyda-Grubbs catalyst second generation; oxalyl dichloride; di-isopropyl azodicarboxylate; palladium 10% on activated carbon; boron trifluoride diethyl etherate; hydrogen; pyridinium p-toluenesulfonate; dimethyl sulfoxide; triethylamine; triphenylphosphine; In tetrahydrofuran; pyridine; hexane; dichloromethane; water; acetic acid; ethyl acetate; toluene; 3.1: Swern oxidation / 3.2: Swern oxidation / 4.2: Wittig reaction / 8.1: Mitsunobu reaction;
DOI:10.1016/j.carres.2011.04.032