benzyl 1-(1-hydroxy-4-phenylbutan-2-ylcarbamoyl)-3-methylbutylcarbamate

Base Information

Chemical Name:benzyl 1-(1-hydroxy-4-phenylbutan-2-ylcarbamoyl)-3-methylbutylcarbamate
CAS No.:1256776-40-5
Molecular Formula:C₂₄H₃₂N₂O₄
Molecular Weight:412.529
Hs Code.:

Synonyms:benzyl 1-(1-hydroxy-4-phenylbutan-2-ylcarbamoyl)-3-methylbutylcarbamate

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Chemical Property of benzyl 1-(1-hydroxy-4-phenylbutan-2-ylcarbamoyl)-3-methylbutylcarbamate

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Technology Process of benzyl 1-(1-hydroxy-4-phenylbutan-2-ylcarbamoyl)-3-methylbutylcarbamate

There total 1 articles about benzyl 1-(1-hydroxy-4-phenylbutan-2-ylcarbamoyl)-3-methylbutylcarbamate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 92.0%

: 1256776-36-9
2-(2-{[(benzyloxy)carbonyl]amino}-4-methylpentanoylamino)-4-phenylbutanoic acid methyl ester

: 1256776-40-5
benzyl 1-(1-hydroxy-4-phenylbutan-2-ylcarbamoyl)-3-methylbutylcarbamate

Guidance literature:: With sodium tetrahydroborate; calcium chloride; In tetrahydrofuran; methanol; for 5h;
DOI:10.1021/jm1009567

Reference yield: 60.0%

: 1256776-40-5
benzyl 1-(1-hydroxy-4-phenylbutan-2-ylcarbamoyl)-3-methylbutylcarbamate

: 1-((1-formyl-3-phenylpropylcarbamoyl)-3-methylbutyl)benzyl carbamate

Guidance literature:: benzyl 1-(1-hydroxy-4-phenylbutan-2-ylcarbamoyl)-3-methylbutylcarbamate; With oxalyl dichloride; dimethyl sulfoxide; In dichloromethane; at -78 ℃; for 0.25h;

With triethylamine; In dichloromethane; at -78 - 0 ℃;
DOI:10.1021/jm1009567

Reference yield:

: 1256776-40-5
benzyl 1-(1-hydroxy-4-phenylbutan-2-ylcarbamoyl)-3-methylbutylcarbamate

: 1256776-26-7
C₃₄H₄₄N₂O₆

Guidance literature:: Multi-step reaction with 2 steps

1.1: oxalyl dichloride; dimethyl sulfoxide / dichloromethane / 0.25 h / -78 °C

1.2: -78 - 0 °C

2.1: ozone / dichloromethane; pentane / -78 - 0 °C

With oxalyl dichloride; ozone; dimethyl sulfoxide; In dichloromethane; pentane; 1.1: Swern oxidation / 1.2: Swern oxidation / 2.1: Griesbaum co-ozonolysis;
DOI:10.1021/jm1009567