[Fe2(μ-CN(Me)(2,6-Me2C6H3))(μ-CO)(CO)(p-NCC6H4CF3)(C5H5)2]O3SCF3

Base Information

Chemical Name:[Fe2(μ-CN(Me)(2,6-Me2C6H3))(μ-CO)(CO)(p-NCC6H4CF3)(C5H5)2]O3SCF3
CAS No.:853416-16-7
Molecular Formula:CF₃O₃S*C₃₀H₂₆F₃Fe₂N₂O₂
Molecular Weight:764.308
Hs Code.:

Synonyms:[Fe2(μ-CN(Me)(2,6-Me2C6H3))(μ-CO)(CO)(p-NCC6H4CF3)(C5H5)2]O3SCF3

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Chemical Property of [Fe2(μ-CN(Me)(2,6-Me2C6H3))(μ-CO)(CO)(p-NCC6H4CF3)(C5H5)2]O3SCF3

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Technology Process of [Fe2(μ-CN(Me)(2,6-Me2C6H3))(μ-CO)(CO)(p-NCC6H4CF3)(C5H5)2]O3SCF3

There total 1 articles about [Fe2(μ-CN(Me)(2,6-Me2C6H3))(μ-CO)(CO)(p-NCC6H4CF3)(C5H5)2]O3SCF3 which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 92.0%

: 306741-65-1
[Fe2(μ-CN(Me)Me2C6H3)(μ-CO)(CO)2(Cp)2]SO3CF3

: 455-18-5
4-CF₃C₆H₄CN

: 853416-16-7
[Fe2(μ-CN(Me)(2,6-Me2C6H3))(μ-CO)(CO)(p-NCC6H4CF3)(C5H5)2]O3SCF3

Guidance literature:: With Me₃NO; In tetrahydrofuran; (N2); Schlenk technique; ligand and Me3NO were added to soln. of Fe complex in THF; soln. was stirred at room temp. for 3 h; solvent removed (vac.); residue washed (Et2O, petroleum ether); filteredthrough Celite with CH2Cl2; elem. anal.;
DOI:10.1016/j.jorganchem.2004.11.006

Reference yield: 60.0%

: 853416-16-7
[Fe2(μ-CN(Me)(2,6-Me2C6H3))(μ-CO)(CO)(p-NCC6H4CF3)(C5H5)2]O3SCF3

: 766-97-2
4-n-methylphenylacetylene

: [Fe(C5H5)(CO)(μ-η2:η2-C[N(Me)(2,6-Me2C6H3)]N=C(C6H3CF3)C=CH(tolyl))Fe(C5H5)(CO)]

Guidance literature:: With n-BuLi; In tetrahydrofuran; hexane; (N2); Schlenk technique; soln. of BuLi in hexane was added to soln. of p-MeC6H4CCH in THF at -50°C; mixt. was stirred at room temp. for 1h; added to soln. of Fe complex in THF at -50°C; mixt. was stirr ed at room temp. for 1 h; filtered through Al2O3; solvent removed (vac.); residue dissolved in CH2Cl2; chromd. (Al2O3, CH2Cl2); elem. anal.;
DOI:10.1016/j.jorganchem.2004.11.006