Potassium; (1S,2R)-1-hydrazinocarbonyl-2-[4-(2-methoxy-ethoxymethoxy)-phenyl]-cyclopropanecarboxylate

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Chemical Name:Potassium; (1S,2R)-1-hydrazinocarbonyl-2-[4-(2-methoxy-ethoxymethoxy)-phenyl]-cyclopropanecarboxylate
CAS No.:117942-46-8
Molecular Formula:C₁₅H₁₉N₂O₆*K
Molecular Weight:362.424
Hs Code.:

Synonyms:Potassium; (1S,2R)-1-hydrazinocarbonyl-2-[4-(2-methoxy-ethoxymethoxy)-phenyl]-cyclopropanecarboxylate

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Chemical Property of Potassium; (1S,2R)-1-hydrazinocarbonyl-2-[4-(2-methoxy-ethoxymethoxy)-phenyl]-cyclopropanecarboxylate

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Technology Process of Potassium; (1S,2R)-1-hydrazinocarbonyl-2-[4-(2-methoxy-ethoxymethoxy)-phenyl]-cyclopropanecarboxylate

There total 5 articles about Potassium; (1S,2R)-1-hydrazinocarbonyl-2-[4-(2-methoxy-ethoxymethoxy)-phenyl]-cyclopropanecarboxylate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 117942-42-4
diethyl 4-<(2-methoxyethoxy)methoxy>benzalmalonate

: 117942-46-8
Potassium; (1S,2R)-1-hydrazinocarbonyl-2-[4-(2-methoxy-ethoxymethoxy)-phenyl]-cyclopropanecarboxylate

Guidance literature:: Multi-step reaction with 3 steps

1: 76 percent / dimethylsulfoxide; tetrahydrofuran / 1.) RT, 1 h, 2.) 50 deg C, 1 h

2: 78 percent / NaOH, H₂O / ethanol / 48 h / Ambient temperature

3: 1.) 5percent KHCO₃, 2.) NH₂NH₂*H₂O / 1.) EtOH, water, 2.) reflux, 24 h

With sodium hydroxide; water; potassium hydrogencarbonate; hydrazine hydrate; In tetrahydrofuran; ethanol; dimethyl sulfoxide;
DOI:10.1021/jo00262a033

Reference yield:

: 117942-43-5
diethyl 2-<4-<(2-methoxyethoxy)methoxy>phenyl>cyclopropane-1,1-dicarboxylate

: 117942-46-8
Potassium; (1S,2R)-1-hydrazinocarbonyl-2-[4-(2-methoxy-ethoxymethoxy)-phenyl]-cyclopropanecarboxylate

Guidance literature:: Multi-step reaction with 2 steps

1: 78 percent / NaOH, H₂O / ethanol / 48 h / Ambient temperature

2: 1.) 5percent KHCO₃, 2.) NH₂NH₂*H₂O / 1.) EtOH, water, 2.) reflux, 24 h

With sodium hydroxide; water; potassium hydrogencarbonate; hydrazine hydrate; In ethanol;
DOI:10.1021/jo00262a033

Reference yield:

: 117942-41-3
4-[(2-methoxyethoxy)methoxy]benzaldehyde

: 117942-46-8
Potassium; (1S,2R)-1-hydrazinocarbonyl-2-[4-(2-methoxy-ethoxymethoxy)-phenyl]-cyclopropanecarboxylate

Guidance literature:: Multi-step reaction with 4 steps

1: 93 percent / piperidine, CH₃COOH / toluene / 12 h / Heating

2: 76 percent / dimethylsulfoxide; tetrahydrofuran / 1.) RT, 1 h, 2.) 50 deg C, 1 h

3: 78 percent / NaOH, H₂O / ethanol / 48 h / Ambient temperature

4: 1.) 5percent KHCO₃, 2.) NH₂NH₂*H₂O / 1.) EtOH, water, 2.) reflux, 24 h

With piperidine; sodium hydroxide; water; potassium hydrogencarbonate; hydrazine hydrate; acetic acid; In tetrahydrofuran; ethanol; dimethyl sulfoxide; toluene;
DOI:10.1021/jo00262a033