2-(1H-indole-3-carbonyl)-N-(3,4,5-trimethoxyphenyl)hydrazinecarbothioamide

Base Information

Chemical Name:2-(1H-indole-3-carbonyl)-N-(3,4,5-trimethoxyphenyl)hydrazinecarbothioamide
CAS No.:1396744-08-3
Molecular Formula:C₁₉H₂₀N₄O₄S
Molecular Weight:400.458
Hs Code.:

Synonyms:2-(1H-indole-3-carbonyl)-N-(3,4,5-trimethoxyphenyl)hydrazinecarbothioamide

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 2-(1H-indole-3-carbonyl)-N-(3,4,5-trimethoxyphenyl)hydrazinecarbothioamide

Chemical Property:

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Technology Process of 2-(1H-indole-3-carbonyl)-N-(3,4,5-trimethoxyphenyl)hydrazinecarbothioamide

There total 3 articles about 2-(1H-indole-3-carbonyl)-N-(3,4,5-trimethoxyphenyl)hydrazinecarbothioamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 91.0%

: 15317-58-5
1H-indole-3-carboxylic acid hydrazide

: 35967-24-9
(3,4,5-trimethoxyphenyl)isothiocyanate

: 1396744-08-3
2-(1H-indole-3-carbonyl)-N-(3,4,5-trimethoxyphenyl)hydrazinecarbothioamide

Guidance literature:: In ethanol; at 60 ℃;
DOI:10.1002/cmdc.201300221

Reference yield:

: 776-41-0
indole-3-carboxylic acid ethyl ester

: 1396744-08-3
2-(1H-indole-3-carbonyl)-N-(3,4,5-trimethoxyphenyl)hydrazinecarbothioamide

Guidance literature:: Multi-step reaction with 2 steps

1: hydrazine hydrate / ethanol / 4 h / Reflux

2: ethanol / 60 °C

With hydrazine hydrate; In ethanol;
DOI:10.1016/j.ejmech.2012.06.047

Reference yield:

: 771-50-6
1H-indole-3-carboxylic acid

: 1396744-08-3
2-(1H-indole-3-carbonyl)-N-(3,4,5-trimethoxyphenyl)hydrazinecarbothioamide

Guidance literature:: Multi-step reaction with 3 steps

1: sulfuric acid / 20 h / Reflux

2: hydrazine hydrate / ethanol / 4 h / Reflux

3: ethanol / 60 °C

With sulfuric acid; hydrazine hydrate; In ethanol;
DOI:10.1016/j.ejmech.2012.06.047