Cp₂Zr[2,5-Me₂-3,4-(mesityl)2C₄]

Base Information

• Chemical Name: Cp₂Zr[2,5-Me₂-3,4-(mesityl)2C₄]
• CAS No.: 1142802-97-8
• Molecular Formula: C₃₄H₃₈Zr
• Molecular Weight: 537.9
• Mol file: 1142802-97-8.mol

Synonyms:Cp₂Zr[2,5-Me₂-3,4-(mesityl)2C₄]

Chemical Property of Cp₂Zr[2,5-Me₂-3,4-(mesityl)2C₄]

Chemical Property:

Purity/Quality:

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Technology Process of Cp₂Zr[2,5-Me₂-3,4-(mesityl)2C₄]

There total 1 articles about Cp₂Zr[2,5-Me₂-3,4-(mesityl)2C₄] which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 50.0%

zirconocene (pyridine)(η2-bis(trimethylsilyl)acetylene) + 1,3,5-trimethyl-2-(prop-1-ynyl)benzene (2114-44-5) → Cp2Zr[2,5-Me2-3,4-(mesityl)2C4] (1142802-97-8)

Guidance literature:

In toluene; byproducts: pyridine, (CH3)3SiC2Si(CH3)3; (N2, Schlenk) the mixt. of 2 equiv of alkyne and Zr-complex in toluene was stirred at room temp. for 16 h; the solvent was removed, the solid was washed with pentane and diethyl ether; elem. anal.;

upstream raw materials:

1,3,5-trimethyl-2-(prop-1-ynyl)benzene

Refernces