16-(4'-(2''-dimethylaminoethoxy)-3'-methoxybenzylidene)-17-oxo-5-androsten-3β-ol

Base Information

Chemical Name:16-(4'-(2''-dimethylaminoethoxy)-3'-methoxybenzylidene)-17-oxo-5-androsten-3β-ol
CAS No.:873113-78-1
Molecular Formula:C₃₁H₄₃NO₄
Molecular Weight:493.687
Hs Code.:

Synonyms:16-(4'-(2''-dimethylaminoethoxy)-3'-methoxybenzylidene)-17-oxo-5-androsten-3β-ol

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Chemical Property of 16-(4'-(2''-dimethylaminoethoxy)-3'-methoxybenzylidene)-17-oxo-5-androsten-3β-ol

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Technology Process of 16-(4'-(2''-dimethylaminoethoxy)-3'-methoxybenzylidene)-17-oxo-5-androsten-3β-ol

There total 1 articles about 16-(4'-(2''-dimethylaminoethoxy)-3'-methoxybenzylidene)-17-oxo-5-androsten-3β-ol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 54.52%

: 53-43-0
dehydroepiandrosterone

: 55589-46-3
4-(2-(dimethylamino)ethoxy)-3-methoxybenzaldehyde

: 873113-78-1
16-(4'-(2''-dimethylaminoethoxy)-3'-methoxybenzylidene)-17-oxo-5-androsten-3β-ol

Guidance literature:: With sodium hydroxide; In methanol; at 20 ℃; for 1h;

Reference yield: 61.83%

: 873113-78-1
16-(4'-(2''-dimethylaminoethoxy)-3'-methoxybenzylidene)-17-oxo-5-androsten-3β-ol

: 16-(4'-(2''-dimethylaminoethoxy)-3'-methoxybenzylidene)-17-oximino-5-androsten-3β-ol

Guidance literature:: With hydroxylamine hydrochloride; sodium acetate; In ethanol; water; for 6h; Heating;

Reference yield:

: 873113-78-1
16-(4'-(2''-dimethylaminoethoxy)-3'-methoxybenzylidene)-17-oxo-5-androsten-3β-ol

: 16-(4'-(2''-dimethylaminoethoxy)-3'-methoxybenzylidene)-17-oximino-5-androsten-3β-yl acetate

Guidance literature:: Multi-step reaction with 2 steps

1: 66.18 percent / pyridine / 2 h / Heating

2: 38.91 percent / hydroxylamine hydrochloride; sodium acetate / H₂O; ethanol / 6 h / Heating

With pyridine; hydroxylamine hydrochloride; sodium acetate; In ethanol; water;