C₃₇H₆₄SSiO₆

Base Information

Chemical Name:C₃₇H₆₄SSiO₆
CAS No.:947769-27-9
Molecular Formula:C₃₇H₆₄O₆SSi
Molecular Weight:665.063
Hs Code.:

C<sub>37</sub>H<sub>64</sub>SSiO<sub>6</sub>

Synonyms:C₃₇H₆₄SSiO₆

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Chemical Property of C₃₇H₆₄SSiO₆

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Technology Process of C₃₇H₆₄SSiO₆

There total 12 articles about C₃₇H₆₄SSiO₆ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 68.0%

: 947769-21-3
C₃₈H₆₄SSiO₄SO₂CH₄

: 947769-27-9
C₃₇H₆₄SSiO₆

Guidance literature:: With water; sodium hydrogencarbonate; methyl iodide; In acetone; at 45 ℃; for 14h;
DOI:10.1021/ol071024e

Reference yield:

: C₁₈H₃₅ISiO

: 947769-27-9
C₃₇H₆₄SSiO₆

Guidance literature:: Multi-step reaction with 7 steps

1.1: 92 percent / Pd(PPh₃)4 / tetrahydrofuran / 14 h / 0 °C

2.1: DIBAL-H / CH₂Cl₂ / 3 h / -78 °C

3.1: 99 percent / CBr₄; 2,6-lutidine; PPh₃ / CH₂Cl₂ / 20 °C

4.1: t-BuLi / diethyl ether; pentane / 0.33 h / -78 - -40 °C

4.2: 72 mg / diethyl ether; pentane / 0.33 h / -78 °C

5.1: 87 percent / LiI; LiAlH₄ / diethyl ether / 0.33 h / -100 °C

6.1: 91 percent / Et₃N; DMAP / CH₂Cl₂ / 3.5 h / 0 - 20 °C

7.1: 68 percent / MeI; NaHCO₃; H₂O / acetone / 14 h / 45 °C

With 2,6-dimethylpyridine; dmap; lithium aluminium tetrahydride; carbon tetrabromide; water; tert.-butyl lithium; diisobutylaluminium hydride; sodium hydrogencarbonate; triethylamine; triphenylphosphine; lithium iodide; methyl iodide; tetrakis(triphenylphosphine) palladium⁽⁰⁾; In tetrahydrofuran; diethyl ether; dichloromethane; acetone; pentane;
DOI:10.1021/ol071024e

Reference yield:

: 947769-16-6
C₂₂H₄₄SiO₂

: 947769-27-9
C₃₇H₆₄SSiO₆

Guidance literature:: Multi-step reaction with 5 steps

1.1: 99 percent / CBr₄; 2,6-lutidine; PPh₃ / CH₂Cl₂ / 20 °C

2.1: t-BuLi / diethyl ether; pentane / 0.33 h / -78 - -40 °C

2.2: 72 mg / diethyl ether; pentane / 0.33 h / -78 °C

3.1: 87 percent / LiI; LiAlH₄ / diethyl ether / 0.33 h / -100 °C

4.1: 91 percent / Et₃N; DMAP / CH₂Cl₂ / 3.5 h / 0 - 20 °C

5.1: 68 percent / MeI; NaHCO₃; H₂O / acetone / 14 h / 45 °C

With 2,6-dimethylpyridine; dmap; lithium aluminium tetrahydride; carbon tetrabromide; water; tert.-butyl lithium; sodium hydrogencarbonate; triethylamine; triphenylphosphine; lithium iodide; methyl iodide; In diethyl ether; dichloromethane; acetone; pentane;
DOI:10.1021/ol071024e