{3-benzyl-2-[4-(tert-butyl-dimethyl-silanyloxy)-benzyl]-3-aza-bicyclo[4.1.0]hept-1-yl}-dimethyl-amine

Base Information

Chemical Name:{3-benzyl-2-[4-(tert-butyl-dimethyl-silanyloxy)-benzyl]-3-aza-bicyclo[4.1.0]hept-1-yl}-dimethyl-amine
CAS No.:882423-31-6
Molecular Formula:C₂₈H₄₂N₂OSi
Molecular Weight:450.74
Hs Code.:

{3-benzyl-2-[4-(<i>tert</i>-butyl-dimethyl-silanyloxy)-benzyl]-3-aza-bicyclo[4.1.0]hept-1-yl}-dimethyl-amine

Synonyms:{3-benzyl-2-[4-(tert-butyl-dimethyl-silanyloxy)-benzyl]-3-aza-bicyclo[4.1.0]hept-1-yl}-dimethyl-amine

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Chemical Property of {3-benzyl-2-[4-(tert-butyl-dimethyl-silanyloxy)-benzyl]-3-aza-bicyclo[4.1.0]hept-1-yl}-dimethyl-amine

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Technology Process of {3-benzyl-2-[4-(tert-butyl-dimethyl-silanyloxy)-benzyl]-3-aza-bicyclo[4.1.0]hept-1-yl}-dimethyl-amine

There total 6 articles about {3-benzyl-2-[4-(tert-butyl-dimethyl-silanyloxy)-benzyl]-3-aza-bicyclo[4.1.0]hept-1-yl}-dimethyl-amine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 252954-28-2
2-benzylamino-3-[4-(tert-butyl-dimethyl-silanyloxy)-phenyl]-propionic acid methyl ester

: 882423-31-6
{3-benzyl-2-[4-(tert-butyl-dimethyl-silanyloxy)-benzyl]-3-aza-bicyclo[4.1.0]hept-1-yl}-dimethyl-amine

Guidance literature:: Multi-step reaction with 3 steps

1: 73 percent / TFA / CHCl₃; methanol

2: 35 percent / Me₃Al / benzene

3: ClTi(O-i-Pr)3; c-C₅H₉MgCl / tetrahydrofuran

With triisopropoxytitanium(IV) chloride; trimethylaluminum; cyclopentylmagnesium chloride; trifluoroacetic acid; In tetrahydrofuran; methanol; chloroform; benzene;
DOI:10.3987/COM-05-S(T)52

Reference yield:

: 882423-23-6
2-(benzyl-but-3-enyl-amino)-3-[4-(tert-butyl-dimethyl-silanyloxy)-phenyl]-propionic acid methyl ester

: 882423-31-6
{3-benzyl-2-[4-(tert-butyl-dimethyl-silanyloxy)-benzyl]-3-aza-bicyclo[4.1.0]hept-1-yl}-dimethyl-amine

Guidance literature:: Multi-step reaction with 2 steps

1: 35 percent / Me₃Al / benzene

2: ClTi(O-i-Pr)3; c-C₅H₉MgCl / tetrahydrofuran

With triisopropoxytitanium(IV) chloride; trimethylaluminum; cyclopentylmagnesium chloride; In tetrahydrofuran; benzene;
DOI:10.3987/COM-05-S(T)52

Reference yield:

: 1080-06-4
L-Tyr-OMe

: 882423-31-6
{3-benzyl-2-[4-(tert-butyl-dimethyl-silanyloxy)-benzyl]-3-aza-bicyclo[4.1.0]hept-1-yl}-dimethyl-amine

Guidance literature:: Multi-step reaction with 5 steps

1: Et₃N; DBU

2: Na(OAc)3BH / 1,2-dichloro-ethane

3: 73 percent / TFA / CHCl₃; methanol

4: 35 percent / Me₃Al / benzene

5: ClTi(O-i-Pr)3; c-C₅H₉MgCl / tetrahydrofuran

With triisopropoxytitanium(IV) chloride; trimethylaluminum; sodium tris(acetoxy)borohydride; cyclopentylmagnesium chloride; 1,8-diazabicyclo[5.4.0]undec-7-ene; triethylamine; trifluoroacetic acid; In tetrahydrofuran; methanol; chloroform; 1,2-dichloro-ethane; benzene;
DOI:10.3987/COM-05-S(T)52