methyl 5-chloro-2-({6-[(4-chlorophenyl)amino]-6-oxohexanoyl}amino)benzoate

Base Information

Chemical Name:methyl 5-chloro-2-({6-[(4-chlorophenyl)amino]-6-oxohexanoyl}amino)benzoate
CAS No.:1103929-62-9
Molecular Formula:C₂₀H₂₀Cl₂N₂O₄
Molecular Weight:423.296
Hs Code.:

Synonyms:methyl 5-chloro-2-({6-[(4-chlorophenyl)amino]-6-oxohexanoyl}amino)benzoate

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Chemical Property of methyl 5-chloro-2-({6-[(4-chlorophenyl)amino]-6-oxohexanoyl}amino)benzoate

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Technology Process of methyl 5-chloro-2-({6-[(4-chlorophenyl)amino]-6-oxohexanoyl}amino)benzoate

There total 5 articles about methyl 5-chloro-2-({6-[(4-chlorophenyl)amino]-6-oxohexanoyl}amino)benzoate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 48.0%

: 5202-89-1
4-chlorobenzenesulfonyl chloride

: 1103929-59-4
6-(4-chlorophenylamino)-6-oxohexanoic acid chloride

: 1103929-62-9
methyl 5-chloro-2-({6-[(4-chlorophenyl)amino]-6-oxohexanoyl}amino)benzoate

Guidance literature:: In N,N-dimethyl acetamide; at 20 ℃; for 17h;
DOI:10.1248/cpb.59.215

Reference yield:

: 1103929-56-1
methyl 6-[(4-chlorophenyl)amino]-6-oxohexanoate

: 1103929-62-9
methyl 5-chloro-2-({6-[(4-chlorophenyl)amino]-6-oxohexanoyl}amino)benzoate

Guidance literature:: Multi-step reaction with 3 steps

1: water; sodium hydroxide / tetrahydrofuran / 2 h / 60 °C

2: thionyl chloride / 1 h / 0 - 20 °C

3: N,N-dimethyl acetamide / 17 h / 20 °C

With thionyl chloride; water; sodium hydroxide; In tetrahydrofuran; N,N-dimethyl acetamide;
DOI:10.1248/cpb.59.215

Reference yield:

: 35444-44-1
methyl adipoyl chloride

: 1103929-62-9
methyl 5-chloro-2-({6-[(4-chlorophenyl)amino]-6-oxohexanoyl}amino)benzoate

Guidance literature:: Multi-step reaction with 4 steps

1: N,N-dimethyl acetamide / 17 h / 0 - 20 °C

2: water; sodium hydroxide / tetrahydrofuran / 2 h / 60 °C

3: thionyl chloride / 1 h / 0 - 20 °C

4: N,N-dimethyl acetamide / 17 h / 20 °C

With thionyl chloride; water; sodium hydroxide; In tetrahydrofuran; N,N-dimethyl acetamide;
DOI:10.1248/cpb.59.215