hepta-5,6-dienoic acid 2-[benzyl-(2,4,6-trimethyl-benzenesulfonyl)-amino]-1-phenyl-propyl ester

Base Information

Chemical Name:hepta-5,6-dienoic acid 2-[benzyl-(2,4,6-trimethyl-benzenesulfonyl)-amino]-1-phenyl-propyl ester
CAS No.:457060-28-5
Molecular Formula:C₃₂H₃₇NO₄S
Molecular Weight:531.716
Hs Code.:

Synonyms:hepta-5,6-dienoic acid 2-[benzyl-(2,4,6-trimethyl-benzenesulfonyl)-amino]-1-phenyl-propyl ester

Suppliers and Price of hepta-5,6-dienoic acid 2-[benzyl-(2,4,6-trimethyl-benzenesulfonyl)-amino]-1-phenyl-propyl ester

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 0 raw suppliers

Chemical Property of hepta-5,6-dienoic acid 2-[benzyl-(2,4,6-trimethyl-benzenesulfonyl)-amino]-1-phenyl-propyl ester

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of hepta-5,6-dienoic acid 2-[benzyl-(2,4,6-trimethyl-benzenesulfonyl)-amino]-1-phenyl-propyl ester

There total 3 articles about hepta-5,6-dienoic acid 2-[benzyl-(2,4,6-trimethyl-benzenesulfonyl)-amino]-1-phenyl-propyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 99.0%

: 187324-63-6
(1R,2S)-2-[N-benzyl-N-(mesitylenesulfonyl)amino]-1-phenyl-1-propanol

: 457060-27-4
hepta-5,6-dienoyl chloride

: 457060-28-5
hepta-5,6-dienoic acid 2-[benzyl-(2,4,6-trimethyl-benzenesulfonyl)-amino]-1-phenyl-propyl ester

Guidance literature:: With pyridine; In dichloromethane; at 20 ℃; for 15h;
DOI:10.1021/ja027148y

Reference yield:

: 73229-30-8
hepta-5,6-diene-1-ol

: 457060-28-5
hepta-5,6-dienoic acid 2-[benzyl-(2,4,6-trimethyl-benzenesulfonyl)-amino]-1-phenyl-propyl ester

Guidance literature:: Multi-step reaction with 3 steps

1: 72 percent / pyridinium dichromate / dimethylformamide / 10 h / 20 °C

2: 81 percent / thionyl chloride / 10 h / 20 °C

3: 99 percent / pyridine / CH₂Cl₂ / 15 h / 20 °C

With pyridine; dipyridinium dichromate; thionyl chloride; In dichloromethane; N,N-dimethyl-formamide;
DOI:10.1021/ja027148y

Reference yield:

: 222167-25-1
hepta-5,6-dienoic acid

: 457060-28-5
hepta-5,6-dienoic acid 2-[benzyl-(2,4,6-trimethyl-benzenesulfonyl)-amino]-1-phenyl-propyl ester

Guidance literature:: Multi-step reaction with 2 steps

1: 81 percent / thionyl chloride / 10 h / 20 °C

2: 99 percent / pyridine / CH₂Cl₂ / 15 h / 20 °C

With pyridine; thionyl chloride; In dichloromethane;
DOI:10.1021/ja027148y