7-Benzyloxy-10-hydroxy-6-methoxy-2,3,10,10a-tetrahydro-9H-1-oxa-3a,9-diaza-benzo[f]azulen-4-one

Base Information

Chemical Name:7-Benzyloxy-10-hydroxy-6-methoxy-2,3,10,10a-tetrahydro-9H-1-oxa-3a,9-diaza-benzo[f]azulen-4-one
CAS No.:129887-08-7
Molecular Formula:C₁₉H₂₀N₂O₅
Molecular Weight:356.378
Hs Code.:

Synonyms:7-Benzyloxy-10-hydroxy-6-methoxy-2,3,10,10a-tetrahydro-9H-1-oxa-3a,9-diaza-benzo[f]azulen-4-one

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Chemical Property of 7-Benzyloxy-10-hydroxy-6-methoxy-2,3,10,10a-tetrahydro-9H-1-oxa-3a,9-diaza-benzo[f]azulen-4-one

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Technology Process of 7-Benzyloxy-10-hydroxy-6-methoxy-2,3,10,10a-tetrahydro-9H-1-oxa-3a,9-diaza-benzo[f]azulen-4-one

There total 3 articles about 7-Benzyloxy-10-hydroxy-6-methoxy-2,3,10,10a-tetrahydro-9H-1-oxa-3a,9-diaza-benzo[f]azulen-4-one which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 129887-05-4
3-(4-Benzyloxy-5-methoxy-2-nitro-benzoyl)-oxazolidine-2-carbaldehyde

: 129887-08-7
7-Benzyloxy-10-hydroxy-6-methoxy-2,3,10,10a-tetrahydro-9H-1-oxa-3a,9-diaza-benzo[f]azulen-4-one

Guidance literature:: With hydrogen; palladium on activated charcoal; In methanol; for 0.25h; under 760 Torr; Ambient temperature;
DOI:10.1039/c39900000874

Reference yield:

: 64154-78-5
4-benzyloxy-5-methoxy-2-nitrobenzoyl chloride

: 129887-08-7
7-Benzyloxy-10-hydroxy-6-methoxy-2,3,10,10a-tetrahydro-9H-1-oxa-3a,9-diaza-benzo[f]azulen-4-one

Guidance literature:: Multi-step reaction with 3 steps

1: pyridine / CH₂Cl₂ / 0.33 h / 0 °C

2: di-isobutylaluminium hydride / toluene / 0.5 h / -78 °C

3: H₂ / 10percent Pd/C / methanol / 0.25 h / 760 Torr / Ambient temperature

With pyridine; diisobutylaluminum hydride; hydrogen; palladium on activated charcoal; In methanol; dichloromethane; toluene;
DOI:10.1039/c39900000874

Reference yield:

: 129887-03-2
3-(4-Benzyloxy-5-methoxy-2-nitro-benzoyl)-oxazolidine-2-carboxylic acid methyl ester

: 129887-08-7
7-Benzyloxy-10-hydroxy-6-methoxy-2,3,10,10a-tetrahydro-9H-1-oxa-3a,9-diaza-benzo[f]azulen-4-one

Guidance literature:: Multi-step reaction with 2 steps

1: di-isobutylaluminium hydride / toluene / 0.5 h / -78 °C

2: H₂ / 10percent Pd/C / methanol / 0.25 h / 760 Torr / Ambient temperature

With diisobutylaluminum hydride; hydrogen; palladium on activated charcoal; In methanol; toluene;
DOI:10.1039/c39900000874