NSP-2,7-(OMHEG)2-2'-(CH₂O[CH₂CH₂O]CH₂CH₂OMe)-6'-Me-AE

Base Information

Chemical Name:NSP-2,7-(OMHEG)2-2'-(CH₂O[CH₂CH₂O]CH₂CH₂OMe)-6'-Me-AE
CAS No.:1031364-57-4
Molecular Formula:C₅₉H₈₉NO₂₅S
Molecular Weight:1244.41
Hs Code.:

NSP-2,7-(OMHEG)2-2'-(CH<sub>2</sub>O[CH<sub>2</sub>CH<sub>2</sub>O]CH<sub>2</sub>CH<sub>2</sub>OMe)-6'-Me-AE

Synonyms:NSP-2,7-(OMHEG)2-2'-(CH₂O[CH₂CH₂O]CH₂CH₂OMe)-6'-Me-AE

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Chemical Property of NSP-2,7-(OMHEG)2-2'-(CH₂O[CH₂CH₂O]CH₂CH₂OMe)-6'-Me-AE

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Technology Process of NSP-2,7-(OMHEG)2-2'-(CH₂O[CH₂CH₂O]CH₂CH₂OMe)-6'-Me-AE

There total 11 articles about NSP-2,7-(OMHEG)2-2'-(CH₂O[CH₂CH₂O]CH₂CH₂OMe)-6'-Me-AE which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: C₆₀H₉₁NO₂₅S

: 1031364-57-4
NSP-2,7-(OMHEG)2-2'-(CH₂O[CH₂CH₂O]CH₂CH₂OMe)-6'-Me-AE

Guidance literature:: With hydrogenchloride; water; for 1.5h; Reflux; Inert atmosphere;

Reference yield:

: 172834-75-2
2,7-dimethoxy acridine-9-carboxylic acid

: 1031364-57-4
NSP-2,7-(OMHEG)2-2'-(CH₂O[CH₂CH₂O]CH₂CH₂OMe)-6'-Me-AE

Guidance literature:: Multi-step reaction with 8 steps

1.1: thionyl chloride / 1 h / Reflux; Inert atmosphere

2.1: pyridine / 37 h / 0 - 20 °C

3.1: boron tribromide / dichloromethane / 48 h / 20 °C

3.2: 20 °C / Cooling with ice

4.1: caesium carbonate / tetrahydrofuran / 4 h / Reflux; Inert atmosphere

5.1: potassium hydroxide; water / 16 h / 20 °C

6.1: pyridine; p-toluenesulfonyl chloride / 0.17 h / 20 °C / Inert atmosphere

6.2: 72 h / 20 °C

7.1: sodium hydrogencarbonate / 1 h / 140 - 150 °C

8.1: hydrogenchloride; water / 1.5 h / Reflux; Inert atmosphere

With pyridine; hydrogenchloride; thionyl chloride; water; boron tribromide; sodium hydrogencarbonate; caesium carbonate; p-toluenesulfonyl chloride; potassium hydroxide; In tetrahydrofuran; dichloromethane;

Reference yield:

: 1031364-44-9
C₁₇H₁₅NO₄

: 1031364-57-4
NSP-2,7-(OMHEG)2-2'-(CH₂O[CH₂CH₂O]CH₂CH₂OMe)-6'-Me-AE

Guidance literature:: Multi-step reaction with 6 steps

1.1: boron tribromide / dichloromethane / 48 h / 20 °C

1.2: 20 °C / Cooling with ice

2.1: caesium carbonate / tetrahydrofuran / 4 h / Reflux; Inert atmosphere

3.1: potassium hydroxide; water / 16 h / 20 °C

4.1: pyridine; p-toluenesulfonyl chloride / 0.17 h / 20 °C / Inert atmosphere

4.2: 72 h / 20 °C

5.1: sodium hydrogencarbonate / 1 h / 140 - 150 °C

6.1: hydrogenchloride; water / 1.5 h / Reflux; Inert atmosphere

With pyridine; hydrogenchloride; water; boron tribromide; sodium hydrogencarbonate; caesium carbonate; p-toluenesulfonyl chloride; potassium hydroxide; In tetrahydrofuran; dichloromethane;