4-<3-phenylisoxazol-5-yl>-6-<3-(3,4,5-trimethoxyphenyl)isoxazol-5-yl>resorcinol

Base Information

Chemical Name:4-<3-phenylisoxazol-5-yl>-6-<3-(3,4,5-trimethoxyphenyl)isoxazol-5-yl>resorcinol
CAS No.:155374-31-5
Molecular Formula:C₂₇H₂₂N₂O₇
Molecular Weight:486.481
Hs Code.:

Synonyms:4-<3-phenylisoxazol-5-yl>-6-<3-(3,4,5-trimethoxyphenyl)isoxazol-5-yl>resorcinol

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Chemical Property of 4-<3-phenylisoxazol-5-yl>-6-<3-(3,4,5-trimethoxyphenyl)isoxazol-5-yl>resorcinol

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Technology Process of 4-<3-phenylisoxazol-5-yl>-6-<3-(3,4,5-trimethoxyphenyl)isoxazol-5-yl>resorcinol

There total 4 articles about 4-<3-phenylisoxazol-5-yl>-6-<3-(3,4,5-trimethoxyphenyl)isoxazol-5-yl>resorcinol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 97.0%

: 155374-30-4
5-(2,4-dihydroxy-5-iodophenyl)-3-phenylisoxazole

: 5-tributylstannyl-3-(3,4,5-trimethoxyphenyl)isoxazole

: 155374-31-5
4-<3-phenylisoxazol-5-yl>-6-<3-(3,4,5-trimethoxyphenyl)isoxazol-5-yl>resorcinol

Guidance literature:: tris-(dibenzylideneacetone)dipalladium⁽⁰⁾; triphenyl-arsane; In 1,4-dioxane; at 50 ℃; for 24h;

Reference yield:

: 41046-68-8
4-iodobenzene-1,3-diol

: 155374-31-5
4-<3-phenylisoxazol-5-yl>-6-<3-(3,4,5-trimethoxyphenyl)isoxazol-5-yl>resorcinol

Guidance literature:: Multi-step reaction with 3 steps

1: 62 percent / 2.5percent bispalladium tris(dibenzylideneacetone) 2(dba)3>, 20percent AsPh₃ / dioxane / 48 h / 50 °C

2: 80 percent / ICl / dioxane / 5 h

3: 97 percent / 2.5percent bispalladium tris(dibenzylideneacetone) 2(dba)3>, 20percent AsPh₃ / dioxane / 24 h / 50 °C

With Iodine monochloride; tris-(dibenzylideneacetone)dipalladium⁽⁰⁾; triphenyl-arsane; In 1,4-dioxane;

Reference yield:

: 155374-29-1
5-(2,4-dihydroxyphenyl)-3-phenylisoxazole

: 155374-31-5
4-<3-phenylisoxazol-5-yl>-6-<3-(3,4,5-trimethoxyphenyl)isoxazol-5-yl>resorcinol

Guidance literature:: Multi-step reaction with 2 steps

1: 80 percent / ICl / dioxane / 5 h

2: 97 percent / 2.5percent bispalladium tris(dibenzylideneacetone) 2(dba)3>, 20percent AsPh₃ / dioxane / 24 h / 50 °C

With Iodine monochloride; tris-(dibenzylideneacetone)dipalladium⁽⁰⁾; triphenyl-arsane; In 1,4-dioxane;