5-[[4-[3-[[(2R)-2-(3-chloro-phenyl)-2-hydroxyethyl]amino]propyl]phenyl]sulfonyl]-2-hydroxybenzamide hydrochloride

Base Information

Chemical Name:5-[[4-[3-[[(2R)-2-(3-chloro-phenyl)-2-hydroxyethyl]amino]propyl]phenyl]sulfonyl]-2-hydroxybenzamide hydrochloride
CAS No.:870103-24-5
Molecular Formula:C₂₄H₂₅ClN₂O₅S*ClH
Molecular Weight:525.453
Hs Code.:

Synonyms:5-[[4-[3-[[(2R)-2-(3-chloro-phenyl)-2-hydroxyethyl]amino]propyl]phenyl]sulfonyl]-2-hydroxybenzamide hydrochloride

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Chemical Property of 5-[[4-[3-[[(2R)-2-(3-chloro-phenyl)-2-hydroxyethyl]amino]propyl]phenyl]sulfonyl]-2-hydroxybenzamide hydrochloride

Chemical Property:

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Technology Process of 5-[[4-[3-[[(2R)-2-(3-chloro-phenyl)-2-hydroxyethyl]amino]propyl]phenyl]sulfonyl]-2-hydroxybenzamide hydrochloride

There total 6 articles about 5-[[4-[3-[[(2R)-2-(3-chloro-phenyl)-2-hydroxyethyl]amino]propyl]phenyl]sulfonyl]-2-hydroxybenzamide hydrochloride which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 2-(benzyloxy)-5-[[4-[3-[[(2R)-2-(3-chloro-phenyl)-2-hydroxyethyl]amino]propyl]phenyl]sulfonyl]-benzamide

: 870103-24-5
5-[[4-[3-[[(2R)-2-(3-chloro-phenyl)-2-hydroxyethyl]amino]propyl]phenyl]sulfonyl]-2-hydroxybenzamide hydrochloride

Guidance literature:: With hydrogen; palladium 10% on activated carbon; In methanol; chlorobenzene; at 20 ℃; for 10h; under 760.051 Torr;

Reference yield:

: 5-[[4-(3-aminopropyl)phenyl]sulfonyl]-2-benzyloxybenzamide

: 870103-24-5
5-[[4-[3-[[(2R)-2-(3-chloro-phenyl)-2-hydroxyethyl]amino]propyl]phenyl]sulfonyl]-2-hydroxybenzamide hydrochloride

Guidance literature:: Multi-step reaction with 2 steps

1.1: N,N'-bis(trimethylsilyl)urea / dimethyl sulfoxide / 1.33 h / 20 - 65 °C

1.2: 40 h / 20 - 65 °C

2.1: hydrogen / palladium 10% on activated carbon / methanol; chlorobenzene / 10 h / 20 °C / 760.05 Torr

With N,N'-bis(trimethylsilyl)urea; hydrogen; palladium 10% on activated carbon; In methanol; dimethyl sulfoxide; chlorobenzene;

Reference yield:

: 2-benzyloxy-5-[[4-[3-(formylamino)propyl]phenyl]-sulfonyl]benzamide

: 870103-24-5
5-[[4-[3-[[(2R)-2-(3-chloro-phenyl)-2-hydroxyethyl]amino]propyl]phenyl]sulfonyl]-2-hydroxybenzamide hydrochloride

Guidance literature:: Multi-step reaction with 3 steps

1.1: hydrogenchloride / methanol / 60 h / 20 °C

2.1: N,N'-bis(trimethylsilyl)urea / dimethyl sulfoxide / 1.33 h / 20 - 65 °C

2.2: 40 h / 20 - 65 °C

3.1: hydrogen / palladium 10% on activated carbon / methanol; chlorobenzene / 10 h / 20 °C / 760.05 Torr

With hydrogenchloride; N,N'-bis(trimethylsilyl)urea; hydrogen; palladium 10% on activated carbon; In methanol; dimethyl sulfoxide; chlorobenzene;