methyl (2S)-2-{4-[1-(4-fluorophenyl)-2-(imidazol-1-yl)ethoxy]-2-(4-fluorophenyl)benzoylamino}-4-methylsulfanylbultyrate

Base Information

Chemical Name:methyl (2S)-2-{4-[1-(4-fluorophenyl)-2-(imidazol-1-yl)ethoxy]-2-(4-fluorophenyl)benzoylamino}-4-methylsulfanylbultyrate
CAS No.:223760-54-1
Molecular Formula:C₃₀H₂₉F₂N₃O₄S*ClH
Molecular Weight:602.102
Hs Code.:

Synonyms:methyl (2S)-2-{4-[1-(4-fluorophenyl)-2-(imidazol-1-yl)ethoxy]-2-(4-fluorophenyl)benzoylamino}-4-methylsulfanylbultyrate

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Chemical Property of methyl (2S)-2-{4-[1-(4-fluorophenyl)-2-(imidazol-1-yl)ethoxy]-2-(4-fluorophenyl)benzoylamino}-4-methylsulfanylbultyrate

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Technology Process of methyl (2S)-2-{4-[1-(4-fluorophenyl)-2-(imidazol-1-yl)ethoxy]-2-(4-fluorophenyl)benzoylamino}-4-methylsulfanylbultyrate

There total 1 articles about methyl (2S)-2-{4-[1-(4-fluorophenyl)-2-(imidazol-1-yl)ethoxy]-2-(4-fluorophenyl)benzoylamino}-4-methylsulfanylbultyrate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 25.0%

: methyl (2S)-2-[2-(4-fluorophenyl)-4-hydroxybenzoylamino]-4-methylsulfanylbutyrate

: 24155-46-2
1-(4-fluorophenyl)-2-(1H-imidazol-1-yl)ethan-1-ol

: 223760-54-1
methyl (2S)-2-{4-[1-(4-fluorophenyl)-2-(imidazol-1-yl)ethoxy]-2-(4-fluorophenyl)benzoylamino}-4-methylsulfanylbultyrate

Guidance literature:: methyl (2S)-2-[2-(4-fluorophenyl)-4-hydroxybenzoylamino]-4-methylsulfanylbutyrate; 1-(4-fluorophenyl)-2-(1H-imidazol-1-yl)ethan-1-ol; With triphenylphosphine; 1,1'-azodicarbonyl-dipiperidine; In tetrahydrofuran; at 20 ℃; for 16h;

With hydrogenchloride; In dichloromethane; at 0 ℃;

Reference yield: 42.0%

: 223760-54-1
methyl (2S)-2-{4-[1-(4-fluorophenyl)-2-(imidazol-1-yl)ethoxy]-2-(4-fluorophenyl)benzoylamino}-4-methylsulfanylbultyrate

: 223759-89-5
(2S)-2-{4-[1-(4-Fluorophenyl)-2-(imidazol-1-yl)ethoxy]-2-(4-fluorophenyl)benzoylamino}-4-methylsulfanylbutyric acid

Guidance literature:: methyl (2S)-2-{4-[1-(4-fluorophenyl)-2-(imidazol-1-yl)ethoxy]-2-(4-fluorophenyl)benzoylamino}-4-methylsulfanylbultyrate; With sodium hydroxide; In methanol; water; at 20 ℃; for 2h;

With hydrogenchloride; pH=7.5;