3-[[bis[[(1,1-dimethylethoxy)carbonyl]amino]methylene]amino]benzylamine

Base Information

Chemical Name:3-[[bis[[(1,1-dimethylethoxy)carbonyl]amino]methylene]amino]benzylamine
CAS No.:1257531-13-7
Molecular Formula:C₁₈H₂₈N₄O₄
Molecular Weight:364.445
Hs Code.:

Synonyms:3-[[bis[[(1,1-dimethylethoxy)carbonyl]amino]methylene]amino]benzylamine

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Chemical Property of 3-[[bis[[(1,1-dimethylethoxy)carbonyl]amino]methylene]amino]benzylamine

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Technology Process of 3-[[bis[[(1,1-dimethylethoxy)carbonyl]amino]methylene]amino]benzylamine

There total 3 articles about 3-[[bis[[(1,1-dimethylethoxy)carbonyl]amino]methylene]amino]benzylamine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 52.7%

: 1257531-12-6
3-[[bis[[(1,1-dimethylethoxy)carbonyl]amino]methylene]amino]benzonitrile

: 1257531-13-7
3-[[bis[[(1,1-dimethylethoxy)carbonyl]amino]methylene]amino]benzylamine

Guidance literature:: With palladium 10% on activated carbon; ammonia; hydrogen; In ethanol; at 20 ℃; for 9h; under 2327.23 Torr;
DOI:10.1021/mp100300k

Reference yield:

: 2237-30-1
m-cyanoaniline

: 1257531-13-7
3-[[bis[[(1,1-dimethylethoxy)carbonyl]amino]methylene]amino]benzylamine

Guidance literature:: Multi-step reaction with 2 steps

1: triethylamine; mercury dichloride / tetrahydrofuran / 2 h / Inert atmosphere

2: palladium 10% on activated carbon; ammonia; hydrogen / ethanol / 9 h / 20 °C / 2327.23 Torr

With palladium 10% on activated carbon; ammonia; hydrogen; triethylamine; mercury dichloride; In tetrahydrofuran; ethanol;
DOI:10.1021/mp100300k

Reference yield:

: 322474-21-5
N,N'-bis-Boc-S-methyl-isothiourea

: 1257531-13-7
3-[[bis[[(1,1-dimethylethoxy)carbonyl]amino]methylene]amino]benzylamine

Guidance literature:: Multi-step reaction with 2 steps

1: triethylamine; mercury dichloride / tetrahydrofuran / 2 h / Inert atmosphere

2: palladium 10% on activated carbon; ammonia; hydrogen / ethanol / 9 h / 20 °C / 2327.23 Torr

With palladium 10% on activated carbon; ammonia; hydrogen; triethylamine; mercury dichloride; In tetrahydrofuran; ethanol;
DOI:10.1021/mp100300k