C₂₅H₂₉N₃OSi

Base Information

Chemical Name:C₂₅H₂₉N₃OSi
CAS No.:1188442-69-4
Molecular Formula:C₂₅H₂₉N₃OSi
Molecular Weight:415.61
Hs Code.:

C<sub>25</sub>H<sub>29</sub>N<sub>3</sub>OSi

Synonyms:C₂₅H₂₉N₃OSi

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Chemical Property of C₂₅H₂₉N₃OSi

Chemical Property:

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Technology Process of C₂₅H₂₉N₃OSi

There total 7 articles about C₂₅H₂₉N₃OSi which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 54.0%

: 1188442-67-2
C₂₀H₂₀IN₃O

: 1066-54-2
trimethylsilylacetylene

: 1188442-69-4
C₂₅H₂₉N₃OSi

Guidance literature:: With diethylamine; bis-triphenylphosphine-palladium(II) chloride; copper(l) iodide; In tetrahydrofuran; at 60 ℃; for 2h;

Reference yield:

: 1188442-31-0
C₉H₁₃BrN₂

: 1188442-69-4
C₂₅H₂₉N₃OSi

Guidance literature:: Multi-step reaction with 5 steps

1.1: tetrahydrofuran / 3 h / Reflux

2.1: n-butyllithium / tetrahydrofuran; hexane / -78 °C / Inert atmosphere

2.2: 5 h / -70 - 20 °C

3.1: potassium tert-butylate / methanol; dimethyl sulfoxide / 15 °C / Inert atmosphere

4.1: n-butyllithium; diisopropylamine / tetrahydrofuran / -70 - -20 °C / Inert atmosphere

4.2: 4 h / -70 - 10 °C

5.1: diethylamine / bis-triphenylphosphine-palladium(II) chloride; copper(l) iodide / tetrahydrofuran / 2 h / 60 °C

With n-butyllithium; potassium tert-butylate; diethylamine; diisopropylamine; bis-triphenylphosphine-palladium(II) chloride; copper(l) iodide; In tetrahydrofuran; methanol; hexane; dimethyl sulfoxide;

Reference yield:

: 1188442-29-6
C₉H₁₁BrN₂O₂

: 1188442-69-4
C₂₅H₂₉N₃OSi

Guidance literature:: Multi-step reaction with 6 steps

1.1: zinc acetate hydrate; hydrogen / platinum(IV) oxide / methanol / 1500.15 Torr / Inert atmosphere

2.1: tetrahydrofuran / 3 h / Reflux

3.1: n-butyllithium / tetrahydrofuran; hexane / -78 °C / Inert atmosphere

3.2: 5 h / -70 - 20 °C

4.1: potassium tert-butylate / methanol; dimethyl sulfoxide / 15 °C / Inert atmosphere

5.1: n-butyllithium; diisopropylamine / tetrahydrofuran / -70 - -20 °C / Inert atmosphere

5.2: 4 h / -70 - 10 °C

6.1: diethylamine / bis-triphenylphosphine-palladium(II) chloride; copper(l) iodide / tetrahydrofuran / 2 h / 60 °C

With n-butyllithium; zinc acetate hydrate; potassium tert-butylate; hydrogen; diethylamine; diisopropylamine; platinum(IV) oxide; bis-triphenylphosphine-palladium(II) chloride; copper(l) iodide; In tetrahydrofuran; methanol; hexane; dimethyl sulfoxide;