6-C-(3-Cyclohexylpropyl)-6-deoxy-1,2:3,4-di-O-isopropylidene-α-D-galactopyranose

Base Information

Chemical Name:6-C-(3-Cyclohexylpropyl)-6-deoxy-1,2:3,4-di-O-isopropylidene-α-D-galactopyranose
CAS No.:174501-79-2
Molecular Formula:C₂₁H₃₆O₅
Molecular Weight:368.514
Hs Code.:

Synonyms:6-C-(3-Cyclohexylpropyl)-6-deoxy-1,2:3,4-di-O-isopropylidene-α-D-galactopyranose

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Chemical Property of 6-C-(3-Cyclohexylpropyl)-6-deoxy-1,2:3,4-di-O-isopropylidene-α-D-galactopyranose

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Technology Process of 6-C-(3-Cyclohexylpropyl)-6-deoxy-1,2:3,4-di-O-isopropylidene-α-D-galactopyranose

There total 3 articles about 6-C-(3-Cyclohexylpropyl)-6-deoxy-1,2:3,4-di-O-isopropylidene-α-D-galactopyranose which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 67.0%

: 701-97-3
cyclohexanepropionic acid

: 174501-67-8
6,7-Dideoxy-1,2:3,4-di-O-isopropylidene-α-D-galacto-octapyranuronic acid

: 174501-79-2
6-C-(3-Cyclohexylpropyl)-6-deoxy-1,2:3,4-di-O-isopropylidene-α-D-galactopyranose

Guidance literature:: With potassium hydroxide; In methanol; at 40 ℃; Kolbe electrolysis: undivided beaker-type glass cells, platinum foils as anode and cathode, 200 mA/cm², cell voltage 30-70 V, 1.1-1.2 F/mol;

Reference yield:

: 71553-88-3
metrhyl (Z)-6,7-dideoxyl-1,2:3,4-di-O-isopropylidene-α-D-galacto-oct-5-enopyranuronate

: 174501-79-2
6-C-(3-Cyclohexylpropyl)-6-deoxy-1,2:3,4-di-O-isopropylidene-α-D-galactopyranose

Guidance literature:: Multi-step reaction with 3 steps

1: 100 percent / H₂ / Pd/C / methanol / Ambient temperature

2: 98 percent / 2 N aq. NaOH / diethyl ether / 2 h / Ambient temperature

3: 67 percent / 1 N KOH / methanol / 40 °C / Kolbe electrolysis: undivided beaker-type glass cells, platinum foils as anode and cathode, 200 mA/cm², cell voltage 30-70 V, 1.1-1.2 F/mol

With potassium hydroxide; sodium hydroxide; hydrogen; palladium on activated charcoal; In methanol; diethyl ether;

Reference yield:

: 174501-68-9
Methyl 6,7-dideoxy-1,2:3,4-di-O-isopropylidene-α-D-galacto-octapyranuronate

: 174501-79-2
6-C-(3-Cyclohexylpropyl)-6-deoxy-1,2:3,4-di-O-isopropylidene-α-D-galactopyranose

Guidance literature:: Multi-step reaction with 2 steps

1: 98 percent / 2 N aq. NaOH / diethyl ether / 2 h / Ambient temperature

2: 67 percent / 1 N KOH / methanol / 40 °C / Kolbe electrolysis: undivided beaker-type glass cells, platinum foils as anode and cathode, 200 mA/cm², cell voltage 30-70 V, 1.1-1.2 F/mol

With potassium hydroxide; sodium hydroxide; In methanol; diethyl ether;