(4R,5S)-4-cyclohexyl-1,5-dimethyl-3-[(1S,2S,3R,4R)-3-methylbicyclo[2.2.1]hept-5-en-2-ylcarbonyl]-2-imidazolidinone

Base Information

Chemical Name:(4R,5S)-4-cyclohexyl-1,5-dimethyl-3-[(1S,2S,3R,4R)-3-methylbicyclo[2.2.1]hept-5-en-2-ylcarbonyl]-2-imidazolidinone
CAS No.:331284-01-6
Molecular Formula:C₂₀H₃₀N₂O₂
Molecular Weight:330.47
Hs Code.:

Synonyms:(4R,5S)-4-cyclohexyl-1,5-dimethyl-3-[(1S,2S,3R,4R)-3-methylbicyclo[2.2.1]hept-5-en-2-ylcarbonyl]-2-imidazolidinone

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Chemical Property of (4R,5S)-4-cyclohexyl-1,5-dimethyl-3-[(1S,2S,3R,4R)-3-methylbicyclo[2.2.1]hept-5-en-2-ylcarbonyl]-2-imidazolidinone

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Technology Process of (4R,5S)-4-cyclohexyl-1,5-dimethyl-3-[(1S,2S,3R,4R)-3-methylbicyclo[2.2.1]hept-5-en-2-ylcarbonyl]-2-imidazolidinone

There total 2 articles about (4R,5S)-4-cyclohexyl-1,5-dimethyl-3-[(1S,2S,3R,4R)-3-methylbicyclo[2.2.1]hept-5-en-2-ylcarbonyl]-2-imidazolidinone which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 62.0%

: 542-92-7,25568-84-7,7313-32-8
cyclopenta-1,3-diene

: 331283-97-7
(4R,5S)-3-[(2E)-2-butenoyl]-4-cyclohexyl-1,5-dimethyl-2-imidazolidinone

: 331284-01-6
(4R,5S)-4-cyclohexyl-1,5-dimethyl-3-[(1S,2S,3R,4R)-3-methylbicyclo[2.2.1]hept-5-en-2-ylcarbonyl]-2-imidazolidinone

Guidance literature:: With diethylaluminium chloride; In dichloromethane; toluene; at -78 ℃; for 3h;

Reference yield:

: 142061-15-2
(4R,5S)-1,5-dimethyl-4-cyclohexyl-2-imidazolidinone

: 331284-01-6
(4R,5S)-4-cyclohexyl-1,5-dimethyl-3-[(1S,2S,3R,4R)-3-methylbicyclo[2.2.1]hept-5-en-2-ylcarbonyl]-2-imidazolidinone

Guidance literature:: Multi-step reaction with 2 steps

1.1: DABCO; copper powder; CuCl / tetrahydrofuran / 0.25 h / 20 °C

1.2: 85 percent / tetrahydrofuran

2.1: 62 percent / Et₂AlCl / CH₂Cl₂; toluene / 3 h / -78 °C

With 1,4-diaza-bicyclo[2.2.2]octane; diethylaluminium chloride; copper; copper(l) chloride; In tetrahydrofuran; dichloromethane; toluene; 1.1: deprotonation / 1.2: Substitution / 2.1: Cycloaddition;