1-(1-isopropyl-6-oxo-1,6-dihydro-3-pyridazinyl)-2-phenyl-1,2-ethanedione

Base Information

• Chemical Name: 1-(1-isopropyl-6-oxo-1,6-dihydro-3-pyridazinyl)-2-phenyl-1,2-ethanedione
• CAS No.: 866262-83-1
• Molecular Formula: C₁₅H₁₄N₂O₃
• Molecular Weight: 270.288

Synonyms:1-(1-isopropyl-6-oxo-1,6-dihydro-3-pyridazinyl)-2-phenyl-1,2-ethanedione

Chemical Property of 1-(1-isopropyl-6-oxo-1,6-dihydro-3-pyridazinyl)-2-phenyl-1,2-ethanedione

Chemical Property:

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Technology Process of 1-(1-isopropyl-6-oxo-1,6-dihydro-3-pyridazinyl)-2-phenyl-1,2-ethanedione

There total 1 articles about 1-(1-isopropyl-6-oxo-1,6-dihydro-3-pyridazinyl)-2-phenyl-1,2-ethanedione which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

2-isopropyl-6-(phenylethynyl)-3(2H)-pyridazinone (524919-41-3) → 1-(1-isopropyl-6-oxo-1,6-dihydro-3-pyridazinyl)-2-phenyl-1,2-ethanedione (866262-83-1)

Guidance literature:

With dimethyl sulfoxide; palladium dichloride; at 140 - 145 ℃; for 3h;

Reference yield:

1-(1-isopropyl-6-oxo-1,6-dihydro-3-pyridazinyl)-2-phenyl-1,2-ethanedione (866262-83-1) + 2,3-diaminomaleonitrile (18514-52-8) → 5-(1-isopropyl-6-oxo-1,6-dihydro-3-pyridazinyl)-6-phenyl-2,3-pyrazinedicarbonitrile (866263-02-7)

Guidance literature:

In acetonitrile; at 70 - 75 ℃; for 3h;

Reference yield:

1-(1-isopropyl-6-oxo-1,6-dihydro-3-pyridazinyl)-2-phenyl-1,2-ethanedione (866262-83-1) + 2-amino-acetamidine dihydrobromide (69816-37-1) → 6-(6-amino-3-phenyl-2-pyrazinyl)-2-isopropyl-3(2H)-pyridazinone

Guidance literature:

With sodium methylate; In methanol; for 1.5h;

upstream raw materials:

2-isopropyl-6-(phenylethynyl)-3(2H)-pyridazinone

Downstream raw materials:

5-(1-isopropyl-6-oxo-1,6-dihydro-3-pyridazinyl)-6-phenyl-2,3-pyrazinedicarbonitrile

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