3,4-cis-7-Methoxy-2,2-dimethyl-3-phenyl-4-(4'-hydroxy-3'-aminophenyl)chroman

Base Information

Chemical Name:3,4-cis-7-Methoxy-2,2-dimethyl-3-phenyl-4-(4'-hydroxy-3'-aminophenyl)chroman
CAS No.:78838-29-6
Molecular Formula:C₂₄H₂₅NO₃*ClH
Molecular Weight:411.928
Hs Code.:

Synonyms:3,4-cis-7-Methoxy-2,2-dimethyl-3-phenyl-4-(4'-hydroxy-3'-aminophenyl)chroman

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Chemical Property of 3,4-cis-7-Methoxy-2,2-dimethyl-3-phenyl-4-(4'-hydroxy-3'-aminophenyl)chroman

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Technology Process of 3,4-cis-7-Methoxy-2,2-dimethyl-3-phenyl-4-(4'-hydroxy-3'-aminophenyl)chroman

There total 2 articles about 3,4-cis-7-Methoxy-2,2-dimethyl-3-phenyl-4-(4'-hydroxy-3'-aminophenyl)chroman which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 65.0%

: 78838-23-0,78838-24-1
3,4-cis-7-Methoxy-2,2-dimethyl-3-phenyl-4-(4'-hydroxy-3'-nitrophenyl)chroman

: 78838-29-6
3,4-cis-7-Methoxy-2,2-dimethyl-3-phenyl-4-(4'-hydroxy-3'-aminophenyl)chroman

Guidance literature:: With hydrogen; palladium on activated charcoal; In methanol; for 1h; under 2585.7 Torr;

Reference yield:

: 51423-18-8
cis-2,2-Dimethyl-3-phenyl-4-(p-hydroxyphenyl)-7-methoxychroman

: 78838-29-6
3,4-cis-7-Methoxy-2,2-dimethyl-3-phenyl-4-(4'-hydroxy-3'-aminophenyl)chroman

Guidance literature:: Multi-step reaction with 2 steps

1: 90 percent / conc. HNO₃ / acetic acid / 0.5 h / 8 - 10 °C

2: 65 percent / H₂ / 10percent Pd/C / methanol / 1 h / 2585.7 Torr

With hydrogen; nitric acid; palladium on activated charcoal; In methanol; acetic acid;

Reference yield:

: 78838-29-6
3,4-cis-7-Methoxy-2,2-dimethyl-3-phenyl-4-(4'-hydroxy-3'-aminophenyl)chroman

: 78838-42-3
4-N-Formyl-6-<4'-(3',4'-cis-7'-methoxy-2',2'-dimethyl-3'-phenyl)chromanyl>dihydrobenz-1,4-oxazine

Guidance literature:: Multi-step reaction with 2 steps

1: K₂CO₃ / acetone

2: 70 percent / K₂CO₃ / 24 h / Heating

With potassium carbonate; In acetone;