4-amino-3,3'-dinitrobenzophenone

Base Information

• Chemical Name: 4-amino-3,3'-dinitrobenzophenone
• CAS No.: 37567-46-7
• Molecular Formula: C₁₃H₉N₃O₅
• Molecular Weight: 287.232
• Mol file: 37567-46-7.mol

Synonyms:4-amino-3,3'-dinitrobenzophenone

Chemical Property of 4-amino-3,3'-dinitrobenzophenone

Chemical Property:

Purity/Quality:

99% ^*data from raw suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of 4-amino-3,3'-dinitrobenzophenone

There total 5 articles about 4-amino-3,3'-dinitrobenzophenone which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 90.9%

3,3'-dinitro-4-chloro benzophenone (37567-44-5) → 4-amino-3,3'-dinitrobenzophenone (37567-46-7)

Guidance literature:

With ammonium hydroxide; In ethanol; at 140 ℃; for 12h;

Reference yield:

3-nitrobenzoic acid (121-92-6) → 4-amino-3,3'-dinitrobenzophenone (37567-46-7)

Guidance literature:

Multi-step reaction with 4 steps

1: thionyl chloride / 3 h / Reflux

2: aluminum (III) chloride / 20 h / 2 °C

3: nitric acid; sulfuric acid / 2 h / 20 °C

4: ammonia; water / methanol / 5 h / Sealed tube; Reflux

With aluminum (III) chloride; thionyl chloride; sulfuric acid; ammonia; water; nitric acid; In methanol; 2: |Friedel-Crafts Acylation;

DOI:10.2174/1570180811666140724184806

Reference yield:

m-nitrobenzoic acid chloride (121-90-4) → 4-amino-3,3'-dinitrobenzophenone (37567-46-7)

Guidance literature:

Multi-step reaction with 3 steps

1: aluminum (III) chloride / 20 h / 2 °C

2: nitric acid; sulfuric acid / 2 h / 20 °C

3: ammonia; water / methanol / 5 h / Sealed tube; Reflux

With aluminum (III) chloride; sulfuric acid; ammonia; water; nitric acid; In methanol; 1: |Friedel-Crafts Acylation;

DOI:10.2174/1570180811666140724184806

upstream raw materials:

3,3'-dinitro-4-chloro benzophenone

3-nitrobenzoic acid

m-nitrobenzoic acid chloride

4-chlorophenyl 3-nitrophenyl ketone

Downstream raw materials:

3,3',4-triaminobenzophenone

(4-amino-3-nitrophenyl)(3-nitrophenyl)methanol

(3-aminophenyl)(3,4-diaminophenyl)methanol

2-(carbomethoxyamino)-5<3-(N¹, N³-dicarbomethoxyguinidino)benzoyl>-1H-benzimidazole