Technology Process of C29H28BrN3O2
There total 7 articles about C29H28BrN3O2 which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
C26H22BrN3O2;
With
boron trifluoride diethyl etherate;
In
tetrahydrofuran; dichloromethane;
at -40 ℃;
for 0.25h;
Inert atmosphere;
allylmagnesium bromide;
In
tetrahydrofuran; dichloromethane;
at -40 - 20 ℃;
for 4h;
DOI:10.1021/ol202475r
- Guidance literature:
-
Multi-step reaction with 6 steps
1.1: toluene / Reflux
2.1: pyridinium perbromide hydrobromide / tetrahydrofuran; chloroform / 2.33 h / -10 °C
3.1: sodium hydride / N,N-dimethyl-formamide; mineral oil / 0 - 20 °C
3.2: 4 h / 0 - 20 °C
4.1: hydrazine hydrate / ethanol / Reflux
5.1: methanol / 24 h / 20 °C
6.1: boron trifluoride diethyl etherate / tetrahydrofuran; dichloromethane / 0.25 h / -40 °C / Inert atmosphere
6.2: 4 h / -40 - 20 °C
With
pyridinium perbromide hydrobromide; boron trifluoride diethyl etherate; sodium hydride; hydrazine hydrate;
In
tetrahydrofuran; methanol; ethanol; dichloromethane; chloroform; N,N-dimethyl-formamide; toluene; mineral oil;
DOI:10.1021/ol202475r
- Guidance literature:
-
Multi-step reaction with 5 steps
1.1: pyridinium perbromide hydrobromide / tetrahydrofuran; chloroform / 2.33 h / -10 °C
2.1: sodium hydride / N,N-dimethyl-formamide; mineral oil / 0 - 20 °C
2.2: 4 h / 0 - 20 °C
3.1: hydrazine hydrate / ethanol / Reflux
4.1: methanol / 24 h / 20 °C
5.1: boron trifluoride diethyl etherate / tetrahydrofuran; dichloromethane / 0.25 h / -40 °C / Inert atmosphere
5.2: 4 h / -40 - 20 °C
With
pyridinium perbromide hydrobromide; boron trifluoride diethyl etherate; sodium hydride; hydrazine hydrate;
In
tetrahydrofuran; methanol; ethanol; dichloromethane; chloroform; N,N-dimethyl-formamide; mineral oil;
DOI:10.1021/ol202475r
