N-[(2E)-3,7-dimethylocta-2,6-dienyl]-N-prop-2-ynyl-(4-toluene)sulfonamide

Base Information

Chemical Name:N-[(2E)-3,7-dimethylocta-2,6-dienyl]-N-prop-2-ynyl-(4-toluene)sulfonamide
CAS No.:913381-16-5
Molecular Formula:C₂₀H₂₇NO₃S
Molecular Weight:361.505
Hs Code.:

Synonyms:N-[(2E)-3,7-dimethylocta-2,6-dienyl]-N-prop-2-ynyl-(4-toluene)sulfonamide

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of N-[(2E)-3,7-dimethylocta-2,6-dienyl]-N-prop-2-ynyl-(4-toluene)sulfonamide

Chemical Property:

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Technology Process of N-[(2E)-3,7-dimethylocta-2,6-dienyl]-N-prop-2-ynyl-(4-toluene)sulfonamide

There total 3 articles about N-[(2E)-3,7-dimethylocta-2,6-dienyl]-N-prop-2-ynyl-(4-toluene)sulfonamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: N-(6-hydroxy-3,7-dimethyl-oct-2-enyl)-4-methyl-N-prop-2-ynyl-benzenesulfonamide

: 913381-16-5
N-[(2E)-3,7-dimethylocta-2,6-dienyl]-N-prop-2-ynyl-(4-toluene)sulfonamide

Guidance literature:: With pyridinium chlorochromate; In dichloromethane; at 20 ℃; for 5h;
DOI:10.1002/anie.200601575

Reference yield:

: 4-methyl-N-(3-methyl-6-oxo-hex-2-enyl)-N-prop-2-ynyl-benzenesulfonamide

: 913381-16-5
N-[(2E)-3,7-dimethylocta-2,6-dienyl]-N-prop-2-ynyl-(4-toluene)sulfonamide

Guidance literature:: Multi-step reaction with 2 steps

1: tetrahydrofuran / 1 h / 20 °C

2: pyridinium chlorochromate / CH₂Cl₂ / 5 h / 20 °C

With pyridinium chlorochromate; In tetrahydrofuran; dichloromethane; 1: Grignard reaction;
DOI:10.1002/anie.200601575

Reference yield:

: 727423-31-6
(E)-N-(3,7-dimethylocta-2,6-dien-1-yl)-4-methyl-N-(prop-2-yn-1-yl)benzenesulfonamide

: 913381-16-5
N-[(2E)-3,7-dimethylocta-2,6-dienyl]-N-prop-2-ynyl-(4-toluene)sulfonamide

Guidance literature:: Multi-step reaction with 3 steps

1.1: AcONa; meta-chloroperbenzoic acid / CH₂Cl₂ / 1 h

1.2: HIO₄*2H₂O / CH₂Cl₂; H₂O / 3 h / 20 °C

2.1: tetrahydrofuran / 1 h / 20 °C

3.1: pyridinium chlorochromate / CH₂Cl₂ / 5 h / 20 °C

With sodium acetate; 3-chloro-benzenecarboperoxoic acid; pyridinium chlorochromate; In tetrahydrofuran; dichloromethane; 2.1: Grignard reaction;
DOI:10.1002/anie.200601575