(E)-2,2,2-trichloro-N-cinnamylacetamide

Base Information

Chemical Name:(E)-2,2,2-trichloro-N-cinnamylacetamide
CAS No.:131120-92-8
Molecular Formula:C₁₁H₁₀Cl₃NO
Molecular Weight:278.565
Hs Code.:

Synonyms:(E)-2,2,2-trichloro-N-cinnamylacetamide

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of (E)-2,2,2-trichloro-N-cinnamylacetamide

Chemical Property:

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Technology Process of (E)-2,2,2-trichloro-N-cinnamylacetamide

There total 1 articles about (E)-2,2,2-trichloro-N-cinnamylacetamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 81.0%

: 59874-81-6
1-(1-imino-2,2,2-trichloroethoxy)-3-phenyl-2(E)-propene

: 131120-92-8
(E)-2,2,2-trichloro-N-cinnamylacetamide

Guidance literature:: With tris-(dibenzylideneacetone)dipalladium⁽⁰⁾; tri-p-tolylphosphite; In dichloromethane; at 20 ℃; for 21h; Schlenk technique; Inert atmosphere;
DOI:10.1055/s-0041-1737140

Reference yield: 58.0%

: 131120-92-8
(E)-2,2,2-trichloro-N-cinnamylacetamide

: 131120-93-9
(5R,6S)-5-Chloro-6-phenyl-2-trichloromethyl-5,6-dihydro-4H-[1,3]oxazine

Guidance literature:: With calcium hypochlorite; carbon dioxide; In diethyl ether; at 20 ℃; for 1h;
DOI:10.1016/S0040-4039(00)97492-6

Reference yield:

: 131120-92-8
(E)-2,2,2-trichloro-N-cinnamylacetamide

: 131120-94-0
(1S,2R)-3-Amino-2-chloro-1-phenyl-propan-1-ol

Guidance literature:: Multi-step reaction with 2 steps

1: 58 percent / aq.Ca(OCl)2, CO₂ / diethyl ether / 1 h / 20 °C

2: 1) aq.HCl 2) 5N aq.NaOH / 1) MeOH, 20 deg C, 1 h 2) 0-5 deg C

With hydrogenchloride; sodium hydroxide; calcium hypochlorite; carbon dioxide; In diethyl ether;
DOI:10.1016/S0040-4039(00)97492-6