Technology Process of C47H62O6SeSi
There total 7 articles about C47H62O6SeSi which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
With
sodium tetrahydroborate;
In
tetrahydrofuran; ethanol;
at 0 - 20 ℃;
for 14h;
Inert atmosphere;
DOI:10.1039/c6ob02268e
- Guidance literature:
-
Multi-step reaction with 4 steps
1.1: sodium hexamethyldisilazane / tetrahydrofuran / 1 h / 0 °C
1.2: 2 h / -78 °C
2.1: Hoveyda-Grubbs catalyst second generation / toluene / Reflux
3.1: N,N,N'N'-tetramethyl-1,3-propanediamine / toluene / 1 h / 0 - 20 °C
4.1: sodium tetrahydroborate / ethanol / 14 h / 0 - 20 °C
With
sodium tetrahydroborate; Hoveyda-Grubbs catalyst second generation; N,N,N'N'-tetramethyl-1,3-propanediamine; sodium hexamethyldisilazane;
In
tetrahydrofuran; ethanol; toluene;
DOI:10.1002/anie.201201383
- Guidance literature:
-
Multi-step reaction with 4 steps
1.1: sodium hexamethyldisilazane / tetrahydrofuran / 1 h / 0 °C
1.2: 2 h / -78 °C
2.1: Hoveyda-Grubbs catalyst second generation / toluene / Reflux
3.1: N,N,N'N'-tetramethyl-1,3-propanediamine / toluene / 1 h / 0 - 20 °C
4.1: sodium tetrahydroborate / ethanol / 14 h / 0 - 20 °C
With
sodium tetrahydroborate; Hoveyda-Grubbs catalyst second generation; N,N,N'N'-tetramethyl-1,3-propanediamine; sodium hexamethyldisilazane;
In
tetrahydrofuran; ethanol; toluene;
DOI:10.1002/anie.201201383