(-)-(1S,2R,4R)-4-(4-methoxybenzyloxy)-2-(4,4-dimethylcyclopent-1-enyl)-2-(hydroxymethyl)cyclobutanol

Base Information

Chemical Name:(-)-(1S,2R,4R)-4-(4-methoxybenzyloxy)-2-(4,4-dimethylcyclopent-1-enyl)-2-(hydroxymethyl)cyclobutanol
CAS No.:960294-57-9
Molecular Formula:C₂₀H₂₈O₄
Molecular Weight:332.44
Hs Code.:

Synonyms:(-)-(1S,2R,4R)-4-(4-methoxybenzyloxy)-2-(4,4-dimethylcyclopent-1-enyl)-2-(hydroxymethyl)cyclobutanol

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of (-)-(1S,2R,4R)-4-(4-methoxybenzyloxy)-2-(4,4-dimethylcyclopent-1-enyl)-2-(hydroxymethyl)cyclobutanol

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Technology Process of (-)-(1S,2R,4R)-4-(4-methoxybenzyloxy)-2-(4,4-dimethylcyclopent-1-enyl)-2-(hydroxymethyl)cyclobutanol

There total 1 articles about (-)-(1S,2R,4R)-4-(4-methoxybenzyloxy)-2-(4,4-dimethylcyclopent-1-enyl)-2-(hydroxymethyl)cyclobutanol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 76.0%

: 960294-70-6
C₄₂H₆₀O₄Si₂

: 960294-57-9
(-)-(1S,2R,4R)-4-(4-methoxybenzyloxy)-2-(4,4-dimethylcyclopent-1-enyl)-2-(hydroxymethyl)cyclobutanol

Guidance literature:: With tetrabutyl ammonium fluoride; In tetrahydrofuran; at 20 ℃;
DOI:10.1002/anie.200702056

Reference yield:

: 960294-57-9
(-)-(1S,2R,4R)-4-(4-methoxybenzyloxy)-2-(4,4-dimethylcyclopent-1-enyl)-2-(hydroxymethyl)cyclobutanol

: 83610-96-2
2-(ethylsulfanylcarbonyl)acetic acid

: 960294-60-4
(+)-(1R,6R,7R,Z)-7-(4-methoxybenzyloxy)-1-(4,4-dimethylcyclopent-1-enyl)-6-hydroxy-5-(hydroxymethylene)-3-oxa-bicyclo[4.2.0]octan-4-one

Guidance literature:: (-)-(1S,2R,4R)-4-(4-methoxybenzyloxy)-2-(4,4-dimethylcyclopent-1-enyl)-2-(hydroxymethyl)cyclobutanol; 2-(ethylsulfanylcarbonyl)acetic acid; In dichloromethane; for 2h; cooling;

With 1-hydroxy-3H-benz[d][1,2]iodoxole-1,3-dione; In dimethyl sulfoxide; at 20 ℃; for 3h;

With triethylsilane; palladium on activated charcoal; In dichloromethane; at 20 ℃; Further stages.;
DOI:10.1002/anie.200702056

Reference yield:

: 960294-57-9
(-)-(1S,2R,4R)-4-(4-methoxybenzyloxy)-2-(4,4-dimethylcyclopent-1-enyl)-2-(hydroxymethyl)cyclobutanol

: 83610-96-2
2-(ethylsulfanylcarbonyl)acetic acid

: 960294-71-7
C₂₅H₃₄O₆S

: 960294-59-1
C₂₅H₃₂O₆S

Guidance literature:: (-)-(1S,2R,4R)-4-(4-methoxybenzyloxy)-2-(4,4-dimethylcyclopent-1-enyl)-2-(hydroxymethyl)cyclobutanol; 2-(ethylsulfanylcarbonyl)acetic acid; In dichloromethane; for 2h; cooling;

With 1-hydroxy-3H-benz[d][1,2]iodoxole-1,3-dione; In dimethyl sulfoxide; at 20 ℃; for 3h; Further stages.;
DOI:10.1002/anie.200702056