11,15,19-tris{N-[2,4,6-(trimethyl)benzenesulfonyl]}-22-{N-[2,4,6-(trimethyl)benzenesulfonyl]-N-[2-(cycloheptyl)methyl]amino}-6-oxo-7,11,15,19-tetraazadocosanohydroxamic acid

Base Information

Chemical Name:11,15,19-tris{N-[2,4,6-(trimethyl)benzenesulfonyl]}-22-{N-[2,4,6-(trimethyl)benzenesulfonyl]-N-[2-(cycloheptyl)methyl]amino}-6-oxo-7,11,15,19-tetraazadocosanohydroxamic acid
CAS No.:868836-39-9
Molecular Formula:C₆₂H₉₄N₆O₁₁S₄
Molecular Weight:1227.73
Hs Code.:

11,15,19-tris{N-[2,4,6-(trimethyl)benzenesulfonyl]}-22-{N-[2,4,6-(trimethyl)benzenesulfonyl]-N-[2-(cycloheptyl)methyl]amino}-6-oxo-7,11,15,19-tetraazadocosanohydroxamic acid

Synonyms:11,15,19-tris{N-[2,4,6-(trimethyl)benzenesulfonyl]}-22-{N-[2,4,6-(trimethyl)benzenesulfonyl]-N-[2-(cycloheptyl)methyl]amino}-6-oxo-7,11,15,19-tetraazadocosanohydroxamic acid

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Chemical Property of 11,15,19-tris{N-[2,4,6-(trimethyl)benzenesulfonyl]}-22-{N-[2,4,6-(trimethyl)benzenesulfonyl]-N-[2-(cycloheptyl)methyl]amino}-6-oxo-7,11,15,19-tetraazadocosanohydroxamic acid

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Technology Process of 11,15,19-tris{N-[2,4,6-(trimethyl)benzenesulfonyl]}-22-{N-[2,4,6-(trimethyl)benzenesulfonyl]-N-[2-(cycloheptyl)methyl]amino}-6-oxo-7,11,15,19-tetraazadocosanohydroxamic acid

There total 7 articles about 11,15,19-tris{N-[2,4,6-(trimethyl)benzenesulfonyl]}-22-{N-[2,4,6-(trimethyl)benzenesulfonyl]-N-[2-(cycloheptyl)methyl]amino}-6-oxo-7,11,15,19-tetraazadocosanohydroxamic acid which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 75.9%

: C₆₂H₉₃N₅O₁₁S₄

: 868836-39-9
11,15,19-tris{N-[2,4,6-(trimethyl)benzenesulfonyl]}-22-{N-[2,4,6-(trimethyl)benzenesulfonyl]-N-[2-(cycloheptyl)methyl]amino}-6-oxo-7,11,15,19-tetraazadocosanohydroxamic acid

Guidance literature:: C₆₂H₉₃N₅O₁₁S₄; With chloroformic acid ethyl ester; triethylamine; In tetrahydrofuran; at 0 ℃; for 0.333333h;

With hydroxylamine; In tetrahydrofuran; methanol; at 20 ℃; for 0.5h;
DOI:10.1021/jm0505009

Reference yield: 75.9%

: 868836-39-9
11,15,19-tris{N-[2,4,6-(trimethyl)benzenesulfonyl]}-22-{N-[2,4,6-(trimethyl)benzenesulfonyl]-N-[2-(cycloheptyl)methyl]amino}-6-oxo-7,11,15,19-tetraazadocosanohydroxamic acid

Guidance literature:

Reference yield:

: 868836-27-5
1-(phthalimido)-4,8,12-tris{N-[2,4,6-(trimethyl)benzenesulfonyl]}-15-N-[2,4,6-(trimethyl)benzenesulfonylamino]-4,8,12-triazapentadecane

: 868836-39-9
11,15,19-tris{N-[2,4,6-(trimethyl)benzenesulfonyl]}-22-{N-[2,4,6-(trimethyl)benzenesulfonyl]-N-[2-(cycloheptyl)methyl]amino}-6-oxo-7,11,15,19-tetraazadocosanohydroxamic acid

Guidance literature:: Multi-step reaction with 5 steps

1.1: NaH / dimethylformamide / 0 °C

1.2: 72.2 percent / dimethylformamide

2.1: hydrazine / methanol / 12 h / Heating

3.1: 70.2 percent / triethylamine / CH₂Cl₂ / 0 - 20 °C

4.1: aq. LiOH / tetrahydrofuran / 0 - 20 °C

5.1: ethyl chloroformate; triethylamine / tetrahydrofuran / 0.33 h / 0 °C

5.2: 75.9 percent / hydroxylamine / methanol; tetrahydrofuran / 0.5 h / 20 °C

With lithium hydroxide; chloroformic acid ethyl ester; sodium hydride; triethylamine; hydrazine; In tetrahydrofuran; methanol; dichloromethane; N,N-dimethyl-formamide;
DOI:10.1021/jm0505009